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192results about How to "The method is easy to operate" patented technology

In-situ power-cut-free welding method for soft mother belts and aluminum bus of cathode of aluminum electrolysis cell

ActiveCN104972220ASolve technical problemsAvoid the defect that exothermic welding cannot be used directlyWelding/cutting media/materialsSoldering mediaExothermic weldingEconomic benefits
The invention relates to the electrolytic aluminum industry, in particular to an in-situ power-cut-free welding method for soft mother belts and an aluminum bus of the cathode of an aluminum electrolysis cell. The method comprises the following steps of 1 in-situ grinding, 2 in-situ fixing, 3 in-situ fusion, 4 pre-welding treatment, 5 preheating, 6 exothermic welding and 7 post-welding treatment. By means of the method, in-situ connection between the soft mother belts and the aluminum bus is directly completed through exothermic welding, the defect that the soft mother belts of a sheet type structure cannot be directly welded in a magnetic field is overcome, the economic benefits of an aluminum electrolysis enterprise are increased, and repairing of the soft mother belts for the aluminum electrolysis enterprise is realized. The operation can be completed under the condition that serial aluminum electrolysis cells are powered all the time, and the repairing purpose can be achieved on the promise of not affecting production of the serial aluminum electrolysis cells. The method is suitable for welding of the soft mother belts and the aluminum bus in various cell types, and is good in universality, easy to operate and high in welding repair efficiency.
Owner:WUHAN UNIV

Method for detecting molecular weight and molecular weight distribution coefficient of medical sodium hyaluronate gel

The invention relates to a method for detecting the weight-average molecular weight and molecular weight distribution coefficient of sodium hyaluronate in medical sodium hyaluronate gel. The method comprises: precisely measuring a proper amount of a medicinal preparation solution, adding a mobile phase to dilute the solution to a to-be-tested sample liquid with the required concentration, performing uniform shaking, performing sample injection, and recording a chromatogram; taking a sodium polystyrenesulfonate reference substance, performing measuring according to the method above, drawing a calibration curve with a GPC software, and using a universal calibration method to obtain weight-average molecular weight and molecular weight distribution coefficient. A laser scattering and gel permeation chromatography combination method is used for detecting the weight-average molecular weight and molecular weight distribution coefficient of sodium hyaluronate in medical sodium hyaluronate gel in the professional standard. The combination method is hard to popularize, for the multi-angle laser light scattering spectrometer is expensive. According to the method, the used device is good in universality, the measurement cost is low, and the result is accurate, reliable and stable.
Owner:ZHEJIANG JINGJIA MEDICAL TECH CO LTD

Method for transplanting silicon nanowire array and preparing simple device thereof

The invention discloses a method for transplanting a silicon nanowire array and preparing a simple device thereof. A multihole silver film prepared on a clean silicon wafer is utilized to act as catalytic metal; the silicon nanowire array is prepared through etching the multihole silver film in hydrofluoric acid or hydrogen peroxide; a silicon-silicon oxide core-shell structure is formed by oxidizing the silicon nanowire array in high-temperature water vapors; the silicon-silicon oxide core-shell structure is placed in a high-temperature aqueous solution of ammonia, and a silicon nanowire array structure detached from a silicon lining is prepared through silicon oxide blocking and silver assisted ammonia water etching. Transplantation of the nanowire array is realized by utilizing a target substrate whose surface is coated by an adhesive material; or an insulating material is used to fix and support the silicon nanowire array and acts as an intermediate insulating layer, the silicon nanowire array is transplanted to a flexible substrate whose surface is coated by a conducting adhesive material, and another layer of a conductive material is covered so as to prepare a simple and flexible breakover circuit device with good ohmic contact. The method disclosed by the invention is simple to operate and low in cost, and can be applied to mass production.
Owner:HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI

Method and apparatus for preparing high-purity gallium

ActiveCN104711438AEffective migrationStabilize the solid-liquid interface regionLiquid stateLiquid metal
The present invention discloses a method and an apparatus for preparing high-purity gallium. According to the method, liquid-state high-purity gallium is placed on the bottom portion of a container and is cooled as a seed crystal, the liquid-state metal gallium is poured into the cooling container to cool and crystallize, a thermal source coil is opened after complete crystallization, the temperature and the movement speed of the thermal source coil are controlled, the thermal source coil moves from bottom to top, the stable solid-liquid interface during the solidification process is ensured, the solidification interception ratio is 70-90%, and the metal gallium can be purified to achieve more than or equal to 6N. The apparatus comprises the cooling container, a constant temperature cold source, the thermal source coil and a control device, wherein the bottom portion of the cooling container is provided with the constant temperature cold source, the upper portion of the cooling container is provided with a dust preventing cover, the thermal source coil sleeves on the outer side of the cooling container, and the thermal source coil is connected with the control device through a conducting wire so as to make the temperature and the movement speed of the thermal source coil be controlled by the control device. According to the present invention, characteristics of simple apparatus mechanism, easy method operation, convenient specification quantifying, good product stability and the like are provided.
Owner:NORTHEASTERN UNIV

Thermal polymerization preparation method of manganides solid solution positive material

The invention relates to a thermal polymerization preparation method of a manganides solid solution positive material. The thermal polymerization preparation method comprises the following steps of: preparing a mixed solution comprising lithium salt, nickel salt and manganese salt according to a general form stoichiometric proportion; adding a thermal polymerization precursor solution to the mixed solution; stirring the mixed solution to polymerize to form a gelatinous material at the temperature of between 80 DEC and 120 DEC and pH of between 4 and 7; drying the obtained gelatinous material in vacuum at the temperature of between 140 DEC and 170 DEC to obtain a resinoid product; pre-burning the resinoid product for 5 to 20 hours at the temperature of between 400 DEC and 700 DEC; carrying out heat preserving on the resinoid product for 5 to 20 hours at the temperature of between 750 DEC and 1000 DEC; and slowly cooling the product to a room temperature after calcination to obtain a finished product. According to the thermal polymerization preparation method, the raw material component blending can reach to molecule degree level, larger nonuniformity of microcosmic material matching ratios by blending with a mechanical method can be avoided; the thermal polymerization preparation method is easy and simple to operate; and the synthetic product is fine and uniform in grain diameter, high in purity, higher in discharge ratio capacity, excellent in circulating performance and high temperature performance and remarkable in magnification performance and can serve as a high power lithium ion battery positive material.
Owner:HEFEI GUOXUAN HIGH TECH POWER ENERGY

Method for removing cyanobacterial bloom and apparatus thereof

The invention discloses a method for removing cyanobacterial bloom, comprising the following steps of: drawing algae-containing water into a curved water channel; breaking bladder of algae in the algae-containing water flowing through the curved water channel by the utilization of supersonic wave so as to make the algae sink and simultaneously breaking the cell wall of the algae in the algae-containing water by the utilization of supersonic wave; inputting the algae-containing water which has undergone ultrasonic treatment during the step 2 into a flocculation reaction tank and carrying out flocculation treatment by the use of a safe flocculating agent; inputting the algae-containing water which has undergone flocculation treatment during the step 3 into a flocculation settler for settlement so as to obtain a sediment and a supernatant; and discharging the supernatant. The invention also discloses an apparatus for removing cyanobacterial bloom. The apparatus contains a water pumping device, an ultrasonic treatment pool, a flocculation stirring pool, a settling basin and a power supply device. The method provided by the invention is easy to operate. The apparatus provided by the invention can be used to remove cyanobacterial bloom more thoroughly and efficiently, effectively purify the algae-containing water and effectively minimize nutrients in water, and can operate without maintenance for a long time.
Owner:INST OF AQUATIC LIFE ACAD SINICA
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