Method for preparing pigment for improving natural colorful silk fibers
A color silk, natural technology, used in dry cleaning fiber products, fiber processing, animal fibers and other directions, can solve the problems of difficult to retain natural pigments, loss of color in natural colored silk fabrics, affecting hygroscopicity, feel and luster, etc. Use value, improve the effect of color
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Embodiment 1
[0017] Embodiment one: natural red silk fiber
[0018] Improve the preparation method of natural color silk fiber pigment, described preparation method method comprises the following steps:
[0019] (1) Raw silk treatment, first soak the natural red silk in a solution containing 5% grafting agent, 1% potassium persulfate, and 30g / L sodium sulfate, the bath ratio is 1:30, and the pH value is adjusted with citric acid is 3, the treatment temperature is 70°C, and the treatment time is 50 minutes;
[0020] (2) steaming, steaming the treated natural red silk with a steamer at a temperature of 100°C for 60 minutes;
[0021] (3), washing for the first time, washing the steamed natural red silk with water;
[0022] (4) Dialdehyde treatment, the natural red silk washed with water for the first time was placed in 0.05% dialdehyde solution, the pH value was adjusted to 3 with citric acid, the treatment temperature was 50°C, and the treatment time was 70 minutes;
[0023] (5), washing ...
Embodiment 2
[0030] Embodiment two: natural yellow silk fiber
[0031] Improve the preparation method of natural color silk fiber pigment, described preparation method method comprises the following steps:
[0032] (1) Raw silk treatment, first soak the natural yellow silk in a solution containing 10% of grafting agent, 3% of potassium persulfate, and 35g / L of sodium sulfate, bath ratio 1:40, and adjust the pH value with citric acid 3, the treatment temperature is 80°C, and the treatment time is 60 minutes;
[0033] (2) steaming, the natural yellow silk after the treatment is steamed with a steamer at a temperature of 110°C for 70 minutes;
[0034] (3), washing for the first time, the natural yellow silk after the steaming is washed with clear water;
[0035] (4) Dialdehyde treatment, the natural yellow silk washed with water for the first time was placed in 1.5% dialdehyde solution, the pH value was adjusted to 3 with citric acid, the treatment temperature was 55°C, and the treatment ti...
Embodiment 3
[0042] Embodiment three: natural green silk fiber
[0043] Improve the preparation method of natural color silk fiber pigment, described preparation method method comprises the following steps:
[0044] (1) Raw silk treatment, first soak the natural green silk in a solution containing 15% grafting agent, 5% potassium persulfate, and 40 g / L sodium sulfate, bath ratio 1:50, and adjust the pH value with citric acid is 3, the treatment temperature is 90°C, and the treatment time is 70 minutes;
[0045] (2), steaming, the natural green silk after the treatment is steamed with a steamer, the temperature is 120°C, and the time is 80 minutes;
[0046] (3), washing for the first time, the natural green silk after the steaming is washed with clear water;
[0047] (4) Dialdehyde treatment, the natural green silk washed for the first time is placed in 2% dialdehyde solution, the pH value is adjusted to 3 with citric acid, the treatment temperature is 60°C, and the treatment time is 80 m...
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