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Preparation method of cutting-free rice and wheat straws by alkaline cooking through vertical digester

A technology of alkaline cooking and vertical pot, which is applied in the field of papermaking, can solve the problems that the cooking liquid cannot be circulated, affects the normal operation of cooking, and cannot use pulping equipment, etc., and achieves good water filtration, reduced power consumption, and reduced loss of stock preparation Effect

Inactive Publication Date: 2013-07-10
KUNMING UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the pulping of grass is easy to bridge or form embolism due to its loose tissue structure, which affects the normal operation of cooking
Moreover, as the cooking progresses, the fragmentation of the forage tends to block the grate, making the cooking liquid unable to circulate, so it cannot be used in the pulping equipment with the vertical pot as the mainstream
Therefore, the cooking vessel selected for rice and wheat straw cooking is either steamed with a low-energy-efficiency steamer, or the horizontal tube continuous digester can only be used to obtain pulp with large fluctuations in quality and poor drainage performance.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] (1) Put the straw from the raw material yard into a trapezoidal groove with a water depth of 80-100 cm. After being soaked in water, the continuously rising belt conveyor will bring the straw in the water onto the belt, and then spray it through the clear water spray irrigation arranged above the belt. , The sprayed straw is sent to the vertical pot via a belt conveyor, and the straw is scattered and distributed to all corners of the pot by a forage distributor that extends vertically into the vertical pot opening with a rotating shaft with a rotating blade, until it reaches the pot opening. , Remove the forage distributor, the valve at the bottom of the pot is half-open to drain the excess free water out of the pot, and the valve is closed; among them, the water after washing the grass materials is clarified, and the obtained sludge is returned to the field, and the obtained clear water is returned to the straw for soaking Pool

[0030] (2) Add the hot alkali solution NaO...

Embodiment 2

[0036] (1) Wash the straw with water;

[0037] (2) Add NaOH and a hot alkali solution with a mass concentration of 20 g / L of anthraquinone to the grass after step (1) washed with water and charged into the vertical pot. The amount of alkali added is 75% of the total amount of alkali used. Add water When the solid-liquid mass ratio is 1:6, the steam of the sealed boiler body heats the material and liquid to 75°C, and the vertical pot liquid medicine circulation and heating system is turned on. After heating to 135°C, the temperature is kept for 30 minutes. Among them, the total alkali consumption is 17% of the rice straw quality, and the anthraquinone consumption is 0.1% of the rice straw quality;

[0038] (3) Step (2) Stop the circulation and heating of the liquid medicine at the end of the cooking and heat preservation, and 85% of the lignin is released. The free black liquor is slowly released from the bottom of the vertical pot, and the valve for emptying the black liquor is clo...

Embodiment 3

[0043] (1) Wash the wheat straw with water.

[0044] (2) Add a mass concentration of 80 g / L sodium hydroxide hot alkali solution to the forage washed in step (1) and put into the vertical pot, add 75% of the total alkali used, and then add water to When the solid-liquid mass ratio is 1:5, the steam is heated to 80°C, the liquid medicine circulation and heating system are turned on, and the cooking temperature is raised to 150°C for 50 minutes. Among them, the total alkali consumption for forage is 20%, and the sulfidity is 20%;

[0045] (3) After the cooking and heat preservation of step (2) is completed, the circulation and heating of the liquid medicine are stopped, and 90% of the lignin is released. That is, the valve at the bottom of the vertical pot is opened to slowly drain the free black liquor out of the pot, and the emptying is closed. Black liquor valve;

[0046] (4) Pump the lye preheated to 150℃, which has not been added in step (2), which accounts for 30% of the total ...

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PUM

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Abstract

The invention provides a preparation method of straw pulp by alkaline cooking through a vertical digester without straw cutting. The preparation method comprises the steps of: washing cutting-free straw raw materials, and putting the straw raw materials into the vertical digester; adding a hot alkali solution, and carrying out liquor circulation cooking by using a conventional sulfate method or caustic soda anthraquinone method; when lignin released by the straw raw materials reaches 80-90% by cooking, discharging free black liquor, supplementing a part of an alkali solution for continuous liquor circulation to the cooking temperature, stopping the liquor circulation, and preserving heat until the cooking is finished; and performing conventional pulp washing, so as to obtain unbleached pulp, and conveying the obtained black liquor to an alkali recovery system. According to the preparation method, the straw materials are not cut, and the liquor circulation is unobstructed and the straw materials are uniformly cooked into the pulp in the vertical digester by utilizing good appearance and maintained characteristics of the straw materials before pulping, so that on the premise of ensuring the quality of cooking, the solid matter concentration of the black liquor can be up to more than 12%, the raw material stock loss can be reduced by about 5%, the cooking capability of unit digester volume can be improved by about 10%, the pulp yield and the viscosity are improved by different degrees, and the level of efficient, energy-saving and clean production of the straw pulp is improved significantly.

Description

Technical field [0001] The invention relates to a method for preparing straw pulp, in particular to a method for preparing straw pulp by directly performing vertical pot cooking without cutting the grass, and belongs to the technical field of papermaking. Background technique [0002] Grass-based raw materials are a huge potential resource of my country's paper industry. In the past, it was used as an important alternative resource for wood to support my country's paper industry for nearly half a century. It's just that the inherent deficiencies of grass fiber raw materials not only restrict the use of high-efficiency energy-saving pulping technology and equipment, but also seriously affect the advancement of clean pulp production. The country had no choice but to restrict the development of straw pulping technology in the late 1990s. Today, the proportion of the straw pulping industry has been reduced to less than 20%. Instead, a large amount of pulp raw materials are imported...

Claims

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Application Information

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IPC IPC(8): D21C1/06D21C1/02D21C5/00
Inventor 陈克利吴初柱朱维
Owner KUNMING UNIV OF SCI & TECH
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