Automatic judgment and control for eluant receiving of buckeye extract
An elution process and automatic judgment technology, applied in chemical instruments and methods, solid adsorbent liquid separation, material analysis through optical means, etc., can solve problems such as poor product quality uniformity, avoid loss and waste, and save labor Costs, effects of avoiding loss and waste
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[0041] Example 1 Rapid Judgment and Automatic Control of the Starting Point and End Point of Collecting the Eluate in the Purification Process of the Macroporous Resin of the Salsa Seed Extract
[0042] Salazi: place of origin: Hanzhong, Shaanxi, storage number: YC1100301;
[0043] Near-infrared spectrometer: Matrix-F, German Bruker Spectroscopy Instrument Co., Ltd.;
[0044] HPLC chromatograph: 1200Series, Agilent Technologies Co., Ltd.;
[0045] Aescin sodium reference substance: batch number 200402, source: China Institute for the Control of Pharmaceutical and Biological Products.
[0046] (1) Construction of near-infrared on-line detection system
[0047] The macroporous resin near-infrared online detection system mainly includes: (1) resin column, (2) flow regulating valve, (3) flow cell, (4) sampling valve, (5) optical fiber, (6) near-infrared spectrometer, (7) ) computer, (8) DCS control system. Among them, the macroporous resin column bypass is equipped with a flow...
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