Phase change heat-conducting thermal silicone grease composition for central processing unit (CPU) radiating and preparation method thereof
A silicone grease composition, phase change heat conduction technology, applied in the direction of heat exchange materials, chemical instruments and methods, etc., can solve the problems of reducing heat dissipation effect, short circuit, large air thermal resistance, etc., and achieve simple preparation process and high heat transfer capacity Strong, high thermal conductivity effect
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[0019] A method for preparing a phase-change heat-conducting silicone grease composition for CPU heat dissipation, comprising the following steps: 1) compounding heat-conducting fillers in particle size: selecting large and medium according to the mass ratio of 10:4.5~1.5:4.5~1.5 1. Thermally conductive fillers with three small particle sizes are mixed in the mixer; the large particle size is 20-30 μm, the medium particle size is 3-19.9 μm, and the small particle size is 50nm-2.9 μm;
[0020] 2) Mix 80-90 mass parts of thermally conductive filler and 1-3 parts of vinyltrimethoxysilane in ethanol after compounding, adjust the pH of the solution to 3-4, and heat to 70-80°C , stirring for 2-4h, removing ethanol to obtain a modified inorganic filler;
[0021] 3) Heat 5-10 parts by mass of paraffin wax (high-precision paraffin wax with a melting point of 50-60°C) to melt, then add 5-10 parts by mass of base oil and the modified inorganic filler prepared in the previous step, and mi...
Embodiment 1
[0025] Weigh 80g of aluminum nitride (spherical, average particle size 20um), 40g of aluminum oxide (spherical, average particle size 10um) and 30g of zinc oxide (average particle size 500nm) into the mixer and mix evenly; Add 1.5g of vinyltrimethoxysilane and 75g of organic solvent ethanol (purity: 95%), mix well, adjust the pH value of the solution to about 3~4 with 37wt% HCl, place it in a 75°C oil bath, and stir for 3h . Dry the product in an oven at 120 °C to remove ethanol to obtain a modified inorganic filler, which is taken out for use.
[0026] Put 10g of Huntz Van-Par high-precision paraffin into a kneader at 70°C to melt, then put 80g of the modified inorganic filler obtained above and 10g of simethicone oil with a viscosity of 500cps into the kneader for 2 h to obtain Finished phase change thermal grease.
[0027] The thermal conductivity of the thermal grease is 7.2 W / m.K.
Embodiment 2
[0029] Weigh 80g of aluminum nitride (spherical, average particle size 20um), 40g of aluminum oxide (spherical, average particle size 10um) and 30g of zinc oxide (average particle size 500nm) into the mixer; then add Mix 3g of vinyltrimethoxysilane and 75g of organic solvent ethanol (purity 95%) evenly, adjust the pH of the solution to about 3~4 with 37wt% HCl, place it in an oil bath at 75°C, and stir for 3h. Dry the product in an oven at 120 °C to remove ethanol to obtain a modified inorganic filler, which is taken out for use.
[0030] Put 10g of Huntz Van-Par high-precision paraffin into a kneader at 70°C to melt, put 80g of the modified thermally conductive filler obtained above, and 8g of simethicone oil with a viscosity of 500cps into the kneader for 2 h to obtain Finished phase change thermal grease.
[0031] The thermal conductivity of the thermal grease is 7.5 W / m.K.
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