High-temperature brazing filler metal for soldering C/C and C/SiC composite materials and preparation methods thereof

A technology of composite materials and high-temperature solder, which is applied in the direction of welding/cutting media/materials, welding equipment, welding media, etc., can solve the problems of low high-temperature strength retention rate of joints and poor joint performance, so as to ensure the mechanical properties of joints, Low cost, good wettability effect

Active Publication Date: 2013-08-14
HARBIN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] The purpose of the present invention is to solve the problem that the existing high-temperature solder for welding C / C or C / SiC has a low joint high-temperature strength retention rate and poor joint performance, and provides a method for brazing C / C and C / SiC composite materials High-temperature solder and its preparation method

Method used

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  • High-temperature brazing filler metal for soldering C/C and C/SiC composite materials and preparation methods thereof

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Effect test

specific Embodiment approach 1

[0018] Specific implementation mode one: the high-temperature brazing material of brazing C / C and C / SiC composite materials in this embodiment is composed of 25-35 parts of Ni, 65-75 parts of Zr or ZrH by weight fraction 2 production.

specific Embodiment approach 2

[0019] Specific embodiment two: the difference between this embodiment and specific embodiment one is that the high-temperature solder for brazing C / C and C / SiC composite materials is composed of 30 parts of Ni, 70 parts of Zr or ZrH by weight fraction 2 production. Others are the same as in the first embodiment.

specific Embodiment approach 3

[0020] Specific embodiment three: the difference between this embodiment and specific embodiment one or two is that the Ni purity is 99.0% to 99.9%, the Zr purity is 99.0% to 99.9%, and the ZrH 2 The purity is 99.0% to 99.9%. Others are the same as in the first or second embodiment.

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Abstract

A high-temperature brazing filler metal for soldering C/C and C/SiC composite materials and preparation methods thereof relate to high-temperature soldering materials and preparation methods of the high-temperature soldering materials and mainly solve the problems of low high-temperature strength retention rate and poor performance of soldering joints in existing high-temperature solders for soldering the C/C and C/SiC composite materials. The high-temperature brazing filler metal for soldering the C/C and C/SiC composite materials is made from Ni and Zr or ZrH2. A method I comprises 1) weighing Ni and Zr or ZrH2, 2) performing smelting to obtain an alloy ingot and 3) performing foil fabrication. A method II comprises 1) weighing Ni and Zr or ZrH2, 2) performing ball milling to obtain a mixed powder and 3) pressing the mixed power to obtain foils and washing and drying the foils. The high-temperature brazing filler metal for soldering the C/C and C/SiC composite materials can provide a good wettability for the C/C and C/SiC composite materials and can mainly be formed into two structures during a soldering process, thereby guaranteeing the mechanical performance of the soldering joints. The components of the high-temperature brazing filler metal for soldering C/C and C/Sic composite materials do not contain precious metals, so that the cost is low; and the melting point of the component Zr is 1852 DEG C, so that the soldering joints can be guaranteed to have a high strength retention rate at 600 DEG C.

Description

technical field [0001] The invention relates to a high-temperature brazing material and a preparation method thereof. Background technique [0002] C / C and C / SiC composite materials have low density, high strength, low ablation rate, high thermal shock resistance, low thermal expansion coefficient, and the strength and modulus increase with temperature within 2000 ° C, so they become Important high-temperature structural materials in the field of aerospace. However, C / C and C / SiC composite materials are difficult to machine and difficult to process into complex shapes, which limits their wide application in practical engineering. Therefore, realizing their connection with themselves or with other materials has important application value. [0003] C / C and C / SiC composite materials have high melting points and cannot form a liquid phase. Common fusion welding methods such as TIG, MIG, laser welding, and electron beam welding are difficult to adapt to the connection of C / C a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B23K35/30B23K35/40
Inventor 张丽霞田成龙雷敏徐李刚田晓羽冯吉才
Owner HARBIN INST OF TECH
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