Preparation method of ceramic substrate
A ceramic substrate and ceramic membrane technology, which is applied in the direction of ceramic layered products, chemical instruments and methods, layered products, etc., can solve the problems of increased manufacturing defect rate, substrate warping, and processing inability, etc.
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[0023] Such as figure 1 Shown, the preparation method of the ceramic substrate of one embodiment, comprises the following steps:
[0024] S10, uniformly mixing the ceramic powder, the first organic binder and the first solvent to obtain a ceramic slurry, then preparing a ceramic film by using the ceramic slurry as a raw material, and finally preparing a ceramic substrate green body by using the ceramic film as a raw material.
[0025] The mass ratio of the ceramic powder, the first organic binder and the first solvent may be 100:30˜45:50˜70.
[0026] The ceramic powder can be Class I porcelain, Class II porcelain or Class III porcelain. Class I ceramics can be C0G characteristic ceramics, etc. Class Ⅱ ceramics can be X7R characteristic ceramics, etc. Class III ceramics can be Z5U characteristic ceramics, etc.
[0027] The first organic binder may be polyvinyl butyral or the like.
[0028] The first solvent may be a mixture of toluene and ethanol, and the mass ratio of tol...
Embodiment 1
[0058] According to the mass ratio of 100:45:70, the C0G characteristic ceramic powder, polyvinyl butyral and a mixture of toluene and ethanol with a mass ratio of 1:1 were mixed and ball milled for 16 hours to obtain a uniform ceramic slurry. The ceramic slurry was cast into a ceramic film with a thickness of 50 µm. Three sheets of 50-micron ceramic membranes are laminated and pressed to obtain laminated and laminated ceramic membranes, and then the laminated and laminated ceramic membranes are cut vertically and horizontally to obtain multiple square ceramic substrate green bodies.
[0059] According to the mass ratio of 100:40:50, zirconia powder, polyvinyl butyral and a mixture of toluene and ethanol with a mass ratio of 1.5:1 were mixed and ball milled for 9 hours to obtain a uniform zirconia slurry. The zirconia slurry was cast to form a zirconia film with a thickness of 30 micrometers. Then cut the zirconia film vertically and horizontally according to the same size as...
Embodiment 2
[0062] According to the mass ratio of 100:30:50, X7R characteristic ceramic powder, polyvinyl butyral and a mixture of toluene and ethanol with a mass ratio of 1.5:1 were mixed and ball milled for 12 hours to obtain a uniform ceramic slurry. The ceramic slurry was cast into a ceramic film with a thickness of 30 µm. Laminate and press eight 30-micron ceramic membranes to obtain laminated and laminated ceramic membranes, and then cut the laminated and laminated ceramic membranes vertically and horizontally to obtain multiple square ceramic substrate green bodies.
[0063] According to the mass ratio of 100:42:47, zirconia powder, polyvinyl butyral and a mixture of toluene and ethanol with a mass ratio of 2:1 were mixed and ball-milled for 10 hours to obtain a uniform zirconia slurry. The zirconia slurry was cast into a zirconia film with a thickness of 40 micrometers. Then cut the zirconia film vertically and horizontally according to the same size as the ceramic substrate gree...
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