Method for preparing ultrafine zeolite powder filling PTFE (polytetrafluoroethylene) composite material
A technology of composite materials and zeolite powder, which is applied in the field of preparation of polytetrafluoroethylene composite materials, can solve the problems of large surface wear of abrasive parts, high hardness of ceramic powder, complex preparation process, etc., and achieve strong market competitiveness and good adsorption , The effect of low friction coefficient
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Embodiment 1
[0036] Embodiment 1, a kind of preparation method of ultrafine zeolite powder filling PTFE composite material, carry out following steps successively:
[0037] 1) Ingredients:
[0038] PTFE (particle size 50μm), 85%,
[0039] Heffield zeolite powder (particle size 0.2μm), 12%,
[0040] Al 2 o 3 (particle size 60nm), 3%,
[0041] 2) Put the mixture prepared in step 1) into a stirrer and stir at a high speed (3500r.p.m) evenly, and then cold press it under 38Mpa strong pressure (that is, press it at room temperature), and the cold pressing time is 3 minute.
[0042] 3) Put the molded product obtained in step 2) into a high-temperature sintering furnace, heat at a heating rate of 80°C / hour, and keep it warm for 30 minutes when the temperature reaches 330°C; then continue to heat at a heating rate of 60°C / hour to 370°C ℃, keep warm for 0.5 hours.
[0043] 4) Cool the sintered product obtained in step 3) to 320°C at a rate of 60°C / hour ℃ for 24 minutes, and then natur...
Embodiment 2
[0045] Embodiment 2, a kind of preparation method of ultrafine zeolite powder filling PTFE composite material, carry out following steps successively:
[0046] 1) Ingredients:
[0047] PTFE (particle size 50μm), 87%,
[0048] Heffield zeolite powder (particle size 0.1μm), 10%,
[0049] Graphite (30μm), 3%,
[0050] 2) Put the mixture prepared in step 1) into the mixer and stir evenly at high speed (3500r.p.m), and then cold press it under 35Mpa strong pressure (that is, press it at room temperature), and the cold pressing time is 3 minute.
[0051] 3) Put the molded product obtained in step 2) into a high-temperature sintering furnace, heat at a heating rate of 30°C / hour, and keep it warm for 30 minutes when the temperature reaches 290°C; then continue heating at a heating rate of 60°C / hour to 375 ℃, keep warm for 0.6 hours.
[0052] 4) Cool the sintered product obtained in step 3) to 290°C at a rate of 60°C / hour and keep it warm for 30 minutes, then naturally cool to room ...
Embodiment 3
[0054] Embodiment 3, a kind of preparation method of ultrafine zeolite powder filling PTFE composite material, carry out following steps successively:
[0055] 1) Ingredients:
[0056] PTFE (particle size 50μm), 90%,
[0057] Mordenite powder (particle size 0.1μm), 9%,
[0058] MoS 2 (particle size 20 nm), 1%,
[0059] 2) Put the mixture prepared in step 1) into the mixer and stir evenly at high speed (3500r.p.m), and then cold press it under 35Mpa strong pressure (that is, press it at room temperature), and the cold pressing time is 5 minute.
[0060] 3) Put the molded product obtained in step 2) into a high-temperature sintering furnace, heat at a heating rate of 60°C / hour, and keep it warm for 0.5 hours when the temperature reaches 285°C; then continue to heat at a heating rate of 60°C / hour to 370 ℃, keep warm for 0.5 hours.
[0061] 4) Cool the sintered product obtained in step 3) to 285°C at a rate of 60°C / hour and keep it warm for 30 minutes, then naturally co...
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