Thoriated tungsten rhenium wire and preparation method thereof
A manufacturing method, the technology of thoriated tungsten, which is applied in the field of thoriated tungsten rhenium wire wound for microwave oven magnetron and its manufacturing field, can solve the problems of low creep resistance, fast growth speed, deformation of microwave oven magnetron, etc., and achieve The grain is not easy to grow and the structure is stable
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[0026] A preparation process of thoriated tungsten-rhenium wire for magnetron coil:
[0027] Step 1: Doping. Pour the thorium nitrate solution, potassium nitrate solution, and aluminum silicate solution into the doping pot and dry the blue tungsten powder through solid-liquid mixing, so that trace elements can be evenly distributed in the blue tungsten powder.
[0028] Step 2: Reduction. The doped blue tungsten powder is reduced in a reduction furnace to obtain thoriated tungsten powder containing trace potassium elements. The reduction adopts a five-stage temperature-controlled reduction process, and the five-stage temperatures are 550°C, 650°C, 750°C, 850°C and 950°C, the holding time of each stage is 60-80min, the loading capacity is 300-350g / boat, the reducing atmosphere is hydrogen, and the flow rate of hydrogen is 3-5m 3 / h, the powder particle size range is 1.3-1.8μm,
[0029] Step 3: Add rhenium, mix the ammonium rhenate solution and the thoriated tungsten powder cont...
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