Method for preparing magnetorheological fluid
A technology of magnetorheological fluid and carrier fluid, applied in the direction of lubricating composition, etc., can solve the problems such as the anti-settling and anti-oxidation properties can not achieve the expected effect, the magnetic saturation strength of magnetic particles is insufficient, the specific gravity is poor, etc., to prevent complexation Agglomeration, enhanced magnetic saturation strength, improved anti-settling effect
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Embodiment 1
[0020] A preparation method of magnetorheological fluid, the specific operation steps are:
[0021] Step 1, dissolving an appropriate amount of carbonyl iron powder particles in a sodium hydroxide solution for chemical cleaning, and then cleaning them in an ultrasonic cleaner for 1 hour to remove impurities on the surface of the carbonyl iron powder particles, then washing the particles with distilled water and drying them. Add the cleaned and dried carbonyl iron powder particles into the nickel sulfate electrolyte, use the nickel plate as the anode, and the carbonyl iron powder as the cathode for electrolytic reaction. The mass ratio of carbonyl iron powder to nickel sulfate is 10:1, and the nickel sulfate solution The concentration is 150g / L, the pH value of the electrolyte is 3.8, the temperature of the electrolytic reaction is 55°C, and the current density is 2A / dm2. Stirring the reaction solution during the reaction can accelerate the reaction and promote the uniformity of...
Embodiment 2
[0027] A preparation method of magnetorheological fluid, the specific operation steps are:
[0028] Step 1, dissolving an appropriate amount of carbonyl iron powder particles in a sodium hydroxide solution for chemical cleaning, and then cleaning them in an ultrasonic cleaner for 1 hour to remove impurities on the surface of the carbonyl iron powder particles, then washing the particles with distilled water and drying them. Add the cleaned and dried carbonyl iron powder particles into the nickel sulfate electrolyte, use the nickel plate as the anode, and the carbonyl iron powder as the cathode for electrolytic reaction. The mass ratio of carbonyl iron powder to nickel sulfate is 8:1, and the nickel sulfate solution The concentration is 300g / L, the pH value of the electrolyte is 5.5, the temperature of the electrolysis reaction is 60°C, and the current density is 5A / dm 2 Stirring the reaction solution during the reaction can speed up the reaction and promote the uniformity of t...
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