Cyclane hydro-conversion catalyst, preparation method and applications
A hydroconversion and catalyst technology, applied in physical/chemical process catalysts, molecular sieve catalysts, chemical instruments and methods, etc., can solve problems such as poor hydrothermal stability, difficult post-treatment processes, etc., to reduce content, reduce synthesis time, Simple preparation method
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0030] (1) Synthesis of Y / Beta / ZSM-12 Composite Molecular Sieve
[0031] Raw material molar ratio: 1.07Na 2 O:8.7SiO 2 :1.5TEABr:0.8NH 4 OH :A1 2 o 3 :100H 2 O. The synthesis process is to weigh sodium hydroxide and TEABr and dissolve them in deionized water according to the above raw material ratio, then add Y-type molecular sieve while stirring, and then add concentrated ammonia water after mixing evenly, stir for half an hour, then add silica sol, and stir for 2 hours Then move to a closed stainless steel reaction kettle. Crystallization at 140° C. for 7 days to obtain a Y / Beta / ZSM-12 composite molecular sieve product.
[0032] (2) Treatment of Y / Beta / ZSM-12 composite molecular sieve
[0033] Take 200 grams of the Y / Beta / ZSM-12 composite molecular sieve prepared in step (1), and exchange it with 400 grams of ammonium nitrate solution with a mass concentration of 50% at 80° C. for 3 times, each time for 2 hours. Dry at 110°C for 6 hours, and calcined at 550°C for 4 ...
Embodiment 2
[0037] The preparation method of catalyst C2 is the same as in Example 1, except that metal Zn and Pt are co-impregnated, and the contents of Pt and Zn are different. The catalyst composition and evaluation results are shown in Table 1.
Embodiment 3
[0039] Take 50 grams of hydrogen-type Y / Beta / ZSM-12 composite molecular sieve prepared in Example 1, 69 grams of SB powder, and 2.50 grams of sage powder, mix well, then add 60ml of deionized water and 2.50ml of concentrated nitric acid (66.5wt%) Fully knead on the roller compactor to make it into a paste-like plastic, extrude a cylindrical strip with a diameter of 1.5mm on the extruder, dry at 110°C for 8 hours, and then bake at 550°C for 4 hours in an air atmosphere to obtain the catalyst carrier D2; An appropriate amount of carrier D2 was impregnated with a solution containing Zn and Pt, then dried at 110°C for 6 hours, and calcined at 500°C for 4 hours in an air atmosphere to obtain catalyst C3. The catalyst composition and evaluation results are shown in Table 1.
PUM
Property | Measurement | Unit |
---|---|---|
specific surface area | aaaaa | aaaaa |
specific surface area | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com