Preparation method for sodium alginate-acrylamide-based hydrogel
A technology of polyacrylamide and sodium alginate, which is applied in the field of polymer materials, can solve the problems of low tensile strength of high-strength hydrogels and low toughness of high-strength double-network hydrogels, and achieve experimental repeatability Strong, easy to operate, broad application prospects
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Embodiment 1
[0016] This embodiment includes the following steps:
[0017] Step 1: Dissolve sodium alginate powder in deionized water in a water bath at 25°C, then add acrylamide monomer, methylenebisacrylamide, ammonium persulfate and N,N,N',N'-tetra Methylethylenediamine, stirred evenly, deionized water accounts for 80% of the total solution mass after mixing; the mass ratio of sodium alginate powder to acrylamide monomer is 1:7.5, and the mass ratio of methylenebisacrylamide to acrylamide monomer The mass ratio is 0.06%, the mass ratio of ammonium persulfate to acrylamide monomer is 0.1%, and the mass ratio of N,N,N',N'-tetramethylethylenediamine to acrylamide monomer is 0.25%; After the prepared solution was left to stand at room temperature for 2 hours, it was poured into a glass mold and heated at 50°C for 3 hours. During this process, the acrylamide monomer was cross-linked into a hydrogel, and the sodium alginate did not cross Linked, but throughout the polyacrylamide hydrogel net...
Embodiment 2
[0021] This embodiment includes the following steps:
[0022] Step 1: Dissolve sodium alginate powder in deionized water in a water bath at 35°C, then add acrylamide monomer, methylene bisacrylamide, ammonium persulfate and N,N,N',N'-tetra Methylethylenediamine, stirred evenly, deionized water accounts for 86% of the total solution mass after mixing; the mass ratio of sodium alginate powder to acrylamide monomer is 1:8, and the mass ratio of methylenebisacrylamide to acrylamide monomer The mass ratio is 0.06%, the mass ratio of ammonium persulfate to acrylamide monomer is 0.1%, and the mass ratio of N,N,N',N'-tetramethylethylenediamine to acrylamide monomer is 0.25%; After the prepared mixture was left to stand at room temperature for 3 hours, it was poured into a glass mold and heated at 50°C for 3 hours. During this process, the acrylamide monomer was crosslinked into a hydrogel, and sodium alginate did not crosslink. Linked, but throughout the polyacrylamide hydrogel netwo...
Embodiment 3
[0026] This embodiment includes the following steps:
[0027] Step 1: Dissolve sodium alginate powder in deionized water in a water bath at 50°C, and then add acrylamide monomer, methylene bisacrylamide, ammonium persulfate and N,N,N',N'-tetra Methylethylenediamine, stirred evenly, deionized water accounts for 88% of the total solution mass after mixing; the mass ratio of sodium alginate powder to acrylamide monomer is 1:9, and the mass ratio of methylenebisacrylamide to acrylamide monomer The mass ratio is 0.06%, the mass ratio of ammonium persulfate to acrylamide monomer is 0.1%, and the mass ratio of N,N,N',N'-tetramethylethylenediamine to acrylamide monomer is 0.25%; After the prepared mixture was left to stand at room temperature for 2 hours, it was poured into a glass mold and heated at 50°C for 3 hours. During this process, the acrylamide monomer was cross-linked into a hydrogel, and sodium alginate did not cross-link Linked, but throughout the polyacrylamide hydrogel ...
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