Preparation method of diamond composite coating of micro milling cutter
A composite coating, diamond technology, applied in metal material coating process, coating, gaseous chemical plating and other directions, to achieve the effect of delaying cracks, reducing processing costs, and improving smoothness
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Embodiment 1
[0029] see figure 1 , using diamond coating equipment for production, the preparation includes the following steps:
[0030] Step a. Load the PCB micro milling cutter 1 into the tooling 2;
[0031] Step b. Install the tooling 2 equipped with the micro milling cutter 1 into the deposition reaction chamber 3;
[0032] Step c. The deposition reaction chamber 3 is evacuated to a vacuum state with a vacuum pump 4;
[0033] step d. Methane (CH 4 ), hydrogen (H 2 ) and oxygen (O 2 ) 3 kinds of gases; among them, the volume ratio of methane, hydrogen and oxygen is (0.1%~10%): (90%~99.99%): (0%~5%);
[0034] Step e. A direct current arc is passed from the power supply 5 to the heating wire installed in the deposition reaction chamber 3; wherein, the heating wire is a tungsten wire or a tantalum wire; the temperature of the heating wire is 2000-2100°C; the applied arc current is 180A;
[0035] step f. In the deposition reaction chamber 3, the deposition process is divided in...
Embodiment 2
[0040] The preparation method of the diamond composite coating of a kind of PCB micro milling cutter of the present invention is similar to embodiment 1, and its difference is:
[0041] step d. Methane CH is introduced into the deposition reaction chamber 4 , hydrogen H 2 and oxygen O 2 Three kinds of gases; among them, the volume ratio of methane, hydrogen and oxygen is (0.1%~10%): (90%~99.99%): (0~6%);
[0042] Step e. Introduce a DC arc to the tungsten wire installed in the deposition reaction chamber; where the temperature of the heating wire is 2100-2200 ° C; the applied arc current is 185A;
[0043] step f. In the deposition reaction chamber, the deposition process is divided into five stages: heating period, nucleation period, submicrocrystalline growth period, ultrafine nanocrystal growth period, and end-of-growth period. The five stages adopt different vapor deposition conditions. The phase and ultrafine nanocrystal growth period can occur cyclically, and the nu...
Embodiment 3
[0048] The preparation method of the diamond composite coating of a kind of PCB micro milling cutter of the present invention is similar to embodiment 1, and its difference is:
[0049] step d. Methane CH is introduced into the deposition reaction chamber 4 , hydrogen H 2 and oxygen O 2 Three kinds of gases; among them, the volume ratio of methane, hydrogen and oxygen is (0.1%~10%): (90%~99.99%): (0~7%);
[0050] Step e. Introduce a direct current arc to the tungsten wire installed in the deposition reaction chamber; among them, the temperature of the heating tungsten wire is 2300°C; the applied arc current is 190A;
[0051] step f. In the deposition reaction chamber, the deposition process is divided into five stages: heating period, nucleation period, submicrocrystalline growth period, ultrafine nanocrystal growth period, and end-growth period. The five stages adopt different atmospheric deposition conditions, and the submicrocrystalline growth The phase and ultrafine ...
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