Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Copper oxide nano-belt and preparation method thereof

A technology of nanobelt and copper oxide, which is applied in the field of nanomaterials and can solve the problems of few reports on copper oxide ribbon

Inactive Publication Date: 2013-12-18
SHENZHEN INSTITUTE OF INFORMATION TECHNOLOGY
View PDF2 Cites 5 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although many literatures have reported on the control of the morphology of the synthesized nano / micro ribbons, there are few reports on the synthesis of nano / micro copper oxide ribbons.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Copper oxide nano-belt and preparation method thereof
  • Copper oxide nano-belt and preparation method thereof
  • Copper oxide nano-belt and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0022] The embodiment of the present invention provides a method for preparing copper oxide nanoribbons with simple process and easy controllable conditions. The preparation method technological process of this copper oxide nanobelt is as follows figure 1 shown, including the following steps:

[0023] Step S01. Prepare the first mixed emulsion of emulsifier and n-hexane: mix the emulsifier and n-hexane and perform emulsification treatment to prepare the first mixed emulsion; wherein, the ratio of emulsifier and n-hexane is 1.5g:60 ~90mL;

[0024] Step S02. Prepare the second mixed emulsion containing copper salt: mix the aqueous solution of copper salt with the first mixed emulsion prepared in step S01, and then perform secondary emulsification treatment to prepare the second mixed emulsion;

[0025] Step S03. Precipitation reaction of copper hydroxide: add water to the second mixed emulsion prepared in step S02 for mixing, and add ammonia water dropwise, adjust the pH of th...

Embodiment 1

[0044] A copper oxide nanobelt and a preparation method thereof. The preparation method is as follows:

[0045] (1) Dissolve 1.5g of Span80 in 72mL of n-hexane, emulsify and mix evenly at a speed of 10000rpm, and record it as the first mixed emulsion;

[0046] (2) Add 18mL of 1.0M CuSO 4 Add the solution to the first mixed emulsion prepared in step (1), continue to emulsify at high speed (10000rpm) for 1min, and record the obtained mixed solution as the second mixed emulsion;

[0047] (3) Quickly add the second mixed emulsion prepared in step (2) to 126mL of deionized water, stir vigorously and dropwise add 0.5M ammonia water to adjust the pH value to about 4, continue stirring for 3 hours, and filter the formed copper hydroxide precipitate, Wash with deionized water and ethanol several times to remove Span80, n-hexane and unreacted raw materials, and dry the washed copper hydroxide precipitate at 80°C for 12 hours in vacuum;

[0048] (4) Calcining the dried copper hydroxid...

Embodiment 2

[0050] A copper oxide nanobelt and a preparation method thereof. The preparation method is as follows:

[0051] Steps (1) to (3) refer to steps (1) to (3) in Example 1;

[0052] Step (4): calcining the dried copper hydroxide precipitate at 600° C. for 0.5-1.0 hour to obtain a copper oxide nanobelt product.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
thicknessaaaaaaaaaa
lengthaaaaaaaaaa
lengthaaaaaaaaaa
Login to View More

Abstract

The invention discloses a copper oxide nano-belt and a preparation method thereof. The preparation method of the copper oxide nano-belt comprises: a step of preparing a first mixed solution of emulsifier and normal hexane, a step of preparing a second mixed solution containing copper salt, a step of carrying out a copper hydroxide precipitation reaction and a step of heat treating copper hydroxide precipitate. In the preparation method of the copper oxide nano-belt, emulsion template technology at room temperature is adopted, the copper salt solution and ammonia water are used as raw materials, precipitation is directly carried out under the action of the emulsion template formed by an oil phase of normal hexane and emulsifier and a water phase to prepare copper hydroxide, and the copper hydroxide is heated to convert into a CUO nano-belt with nano holes. The preparation method is low in necessary temperature, simple and convenient to operate, good in reproducibility, high in yield and low in cost, and the size and morphology of the copper oxide nano-belt can be controlled by regulating and controlling the reaction conditions. The nano holes are distributed on the surface of the prepared prepared copper oxide nano-belt, thereby having large specific surface area and excellent physical and chemical properties on the surface.

Description

technical field [0001] The invention belongs to the technical field of nanomaterials, and in particular relates to a copper oxide nanobelt and a preparation method thereof. Background technique [0002] Due to their wide application in functional materials such as catalysis, photolysis, and electromagnetic materials, transition metal oxides have become an important research object for material scientists. Copper oxide is a very good P-type semiconductor, its bandgap value is 1.85eV, as a kind of important transition metal oxide, after the size reaches nanoscale, because of its large specific surface area and excellent surface physical and chemical properties , such as: very large interface and specific surface area, uniformity and high surface activity, unusual optical, electrical, magnetic and catalytic properties, making it useful in solar cells, microelectronic devices, magnetic storage, gas catalysis, gas sensing There are many potential applications in sensors and othe...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C01G3/02B82Y30/00
Inventor 刘白刘力睿
Owner SHENZHEN INSTITUTE OF INFORMATION TECHNOLOGY
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com