Sn-Ag-Cu system lead-free soldering paste
A lead-free solder paste and flux technology, applied in the direction of welding medium, welding equipment, welding/cutting medium/material, etc., can solve the problems of function deterioration, unusability, thermal damage of electronic parts, etc., and achieve the effect of long pot life
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example 1
[0032] Example 1 is according to the present invention and a comparative example, in which the flux is prepared using maleic rosin, polymerized rosin, hydrogenated rosin and phenol-modified rosin. Flux is made by adding rosin to a solvent and heating it to melt the rosin. The heating was then turned off and cooled to about 100°C. When the temperature of the liquid reaches about 100°C, the thixotropic agent is added and melted, followed by the activator and stirred to dissolve. After all the materials are dissolved, the flux is solidified by water cooling or isocooling.
example 2
[0033] Example 2 is mixing Sn-Ag based solder powder with the flux prepared in Example 1 to prepare solder paste. The flux content of each solder paste is a reference value of 10.5% (mass), and the flux content can be adjusted until the viscosity is about 200 Pa per second. Each solder paste was left at room temperature for one day, and then its viscosity was measured. In addition, each solder paste was preserved for 60 days in a storage room set at a constant temperature of 25° C., and then its viscosity was measured. The change over time of each solder paste can be compared and pot life can be determined.
example 3
[0034] Example 3 is a comparison of the wettability and color 2 of the solder paste residue produced in Example 2. Measure the temperature of the solder bath to be 250+3°C. The color of the solder paste residue is determined by the printed solder paste. Printed using a metal mask with a thickness of 0.2mm and a hole with a diameter of 6.5mm on a tough copper plate measuring 5.0mm x 10.0mm x 0.5mm and then reflowed using a solder bath at 250+3°C . The color of the flux residue can be compared after cooling.
[0035] Summarizing the above, the solder powder of the alloy has at least 1% by mass of Sb added to the Sn-Ag alloy or Sn-Ag-Cu-based alloy, thereby suppressing the change in viscosity when maleic rosin is used. However, when the Sb content is less than 1% by mass, it cannot suppress the change in viscosity, and when the addition of Sb exceeds 8% by mass, the wettability of the solder paste will be inhibited. Furthermore, according to the present invention, i...
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