Preparation method for thermal-barrier coating
A technology of thermal barrier coating and bonding layer, applied in the field of metal surface treatment, can solve the problem that the oxidation resistance of thermal barrier coating is not improved, etc.
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Embodiment 1
[0026] The nickel-based superalloy K4169 is used as the substrate, and a sample of 10×10×3mm is processed by wire cutting. Use gasoline and alcohol to carry out oily ultrasonic cleaning on the sample in sequence, and use corundum grit to sandblast the surface of the sample under the pressure of 0.1 MPa; use cold spray to prepare a NiCoCrAlYTa bonding layer with a thickness of 50 μm on the surface of the sandblasted sample, The spraying parameters are 25L / h of gasoline, 900L / min of oxygen, and 400mm of spraying distance; use atmospheric plasma spraying to prepare ZrO with a thickness of 100μm on the bonding layer 2 -7wt.Y 2 o 3 Ceramic layer, spraying power 43kW, Ar 60×10 -3 m 3 min -1 , H 2 4×10 -3 m 3 min -1 , spraying distance 110mm; use magnetron target current 2A, bias voltage 150V, air pressure 4×10 -3 Pa, prepare an aluminum film with a thickness of 5 μm on the surface of the ceramic layer; keep it at 700°C for 2h, keep it at 1100°C for 4h, the heating rate is ...
Embodiment 2
[0028]The low-activation steel 316L is used as the substrate, and the sample of 10×10×3mm is processed by wire cutting. Use gasoline and alcohol to clean the sample with oil stains ultrasonically in sequence, and use corundum grit to sandblast the surface of the sample at a pressure of 0.2 MPa; use supersonic flame spraying to prepare a NiAl bond with a thickness of 50 μm on the surface of the sandblasted sample layer, the amount of sprayed gasoline is 25L / h, the amount of oxygen is 900L / min, and the spraying distance is 400mm; use atmospheric plasma spraying to prepare ZrO with a thickness of 150μm on the bonding layer 2 -7wt.Y 2 o 3 Ceramic layer, spraying power 43kW, Ar 60×10 -3 m 3 min -1 , H 2 4×10 -3 m 3 min -1 , spraying distance 110mm; use magnetron target current 2A, bias voltage 150V, air pressure 3×10 -3 Pa, prepare an aluminum film with a thickness of 10 μm on the surface of the ceramic layer; keep it at 700°C for 2h, keep it at 1100°C for 4h, the heating...
Embodiment 3
[0030] The low-activation steel 316L is used as the substrate, and the sample of 10×10×3mm is processed by wire cutting. Use gasoline and alcohol to clean the sample with oil stains ultrasonically in sequence, and use corundum grit to sandblast the surface of the sample under 0.3 MPa pressure; use atmospheric plasma spraying to prepare a NiAl bonding layer with a thickness of 50 μm on the surface of the sandblasted sample , the amount of gasoline sprayed is 25L / h, the amount of oxygen is 900L / min, and the spraying distance is 400mm; use atmospheric plasma spraying to prepare ZrO with a thickness of 200μm on the bonding layer 2 -7wt.Y 2 o 3 Ceramic layer, spraying power 43kW, Ar 60×10 -3 m 3 min -1 , H 2 4×10 -3 m 3 min -1 , spraying distance 110mm; use magnetron target current 2A, bias voltage 150V, air pressure 4×10 -3 Pa, prepare an aluminum film with a thickness of 15 μm on the surface of the ceramic layer; keep it at 700°C for 2h, keep it at 1100°C for 4h, the he...
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