Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

A kind of preparation method of nano silver wire

A nano-silver wire and nano-fiber technology, used in nanotechnology, filament/wire forming, textiles and papermaking, etc., can solve the problem of flexible optoelectronic materials with poor resistance uniformity and bending, long equipment process, and nano-silver wire. Poor uniformity and other problems, to achieve the effect of being conducive to stable implementation, good spinnability and good shape

Active Publication Date: 2016-02-03
ANHUI JINGZHUO OPTICAL DISPLAY TECH CO LTD
View PDF8 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the above methods have their own characteristics, to a certain extent, there are problems such as less preparation, high cost, expensive equipment and long process, especially the uniformity of silver nanowires prepared by the above methods. Poor stability, uncontrollable diameter and length, resulting in poor resistance uniformity and bendability of flexible optoelectronic materials prepared from it

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A kind of preparation method of nano silver wire
  • A kind of preparation method of nano silver wire
  • A kind of preparation method of nano silver wire

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] 1. Preparation of spinning solution

[0035] Dissolve analytically pure silver nitrate in pure water, stir and mix, and prepare a silver nitrate solution with a concentration of 30% by mass;

[0036] Take 100ml of the above silver nitrate solution, add 5g of polyvinylpyrrolidone with a weight average molecular weight of 80,000 to it, stir, after the polyvinylpyrrolidone is dissolved, add butyl titanate with a volume ratio of 1:1 to the silver nitrate solution 4ml of the mixed solution with acetylacetone, continue to stir until the ingredients are fully dissolved and mixed, and then stand still until the bubbles disappear completely to prepare a spinning solution.

[0037] 2. Preparation of nanofibers

[0038] Add the above-mentioned spinning solution to the feeding device of the electrospinning equipment, set the spinning voltage to 15kV, the feeding rate of the spinning solution (that is, the spinning rate) to 20ul / min, and the receiving distance to 8cm for electrostatic spinn...

Embodiment 2

[0043] 1. Preparation of spinning solution

[0044] Dissolve analytically pure silver nitrate in pure water, stir and mix, and prepare a silver nitrate solution with a concentration of 30% by mass;

[0045] Take 100ml of the above silver nitrate solution, add 10g of polyvinylpyrrolidone with a weight average molecular weight of 100,000 to it, stir, and after the polyvinylpyrrolidone is dissolved, add butyl titanate with a volume ratio of 1:2 to the silver nitrate solution Mix 6 ml of the mixed solution with acetylacetone, continue to stir until the ingredients are fully dissolved and mixed, and then stand still until the bubbles disappear completely to prepare a spinning solution.

[0046] 2. Preparation of nanofibers

[0047] Add the above-mentioned spinning solution to the feeding device of the electrospinning equipment, set the spinning voltage to 17kV, the feeding rate of the spinning solution to be 30ul / min, and the receiving distance to be 13cm, and perform electrospinning to ob...

Embodiment 3

[0051] 1. Preparation of spinning solution

[0052] Dissolve analytically pure silver nitrate in pure water, stir and mix, and prepare a silver nitrate solution with a concentration of 35% by mass;

[0053] Take 100ml of the silver nitrate solution, add 3g of polyvinylpyrrolidone with a weight average molecular weight of 500,000 to it, stir, and after the polyvinylpyrrolidone is dissolved, add butyl titanate with a volume ratio of 1:1 to the silver nitrate solution Mix 6 ml of the mixed solution with acetylacetone, continue to stir until the ingredients are fully dissolved and mixed, and then stand still until the bubbles disappear completely to prepare a spinning solution.

[0054] 2. Preparation of nanofibers

[0055] Add the above-mentioned spinning solution to the feeding device of the electrospinning equipment, set the spinning voltage to 10kV, the feeding rate of the spinning solution to 60ul / min, and the receiving distance to be 5cm. Electrospinning is performed to obtain nanof...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
diameteraaaaaaaaaa
diameteraaaaaaaaaa
diameteraaaaaaaaaa
Login to View More

Abstract

The invention provides a method for preparing nanometer silver wires. The method includes the following steps of firstly, dissolving water-soluble high molecular polymers in a silver salt solution, and then adding an additive into the solution to obtain a spinning solution; secondly, conducting electrostatic spinning on the spinning solution to obtain nanometer fibers; thirdly, conducting deoxidation on the nanometer fibers to obtain the nanometer silver wires. The additive comprises butyl titanate and acetylacetone, wherein the volume ratio of the butyl titanate to the acetylacetone is 1:0.5-5. The method is easy to operate and high in controllability, and the nanometer silver wires prepared through the method are the same in size, excellent in bending resistance performance and capable of being widely applied to various transparent conducting materials.

Description

Technical field [0001] The invention belongs to the technical field of nano material preparation, and specifically relates to a preparation method of nano silver wires. Background technique [0002] As a nano-scale wire, nanowire is a one-dimensional structure that is limited to 100 nanometers or less in the horizontal direction (there is no limitation in the vertical direction). In addition to the excellent electrical conductivity of silver, nano-silver wires also have excellent light transmittance and bending resistance due to the nano-level size effect, so they are considered to be the most likely alternative to traditional indium tin oxide (ITO) The material of the transparent electrode. Compared with traditional ITO transparent conductive materials, nano-silver wires have the advantages of low consumption and low price, so they can be widely used in various transparent conductive materials, such as flexible solar cells, capacitive screen conductive materials, etc., so as to...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): B22F9/24B82Y40/00D01D5/00
Inventor 周志华
Owner ANHUI JINGZHUO OPTICAL DISPLAY TECH CO LTD
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com