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Linking agent, organic ceramic material, organic ceramic circuit board and preparation method thereof

A technology of organic ceramics and ceramic materials, used in printed circuit manufacturing, circuit substrate materials, printed circuits, etc., can solve the problems of limited wire width-to-depth ratio, low peel strength, low thermal conductivity of finished products, etc., to improve thermal conductivity, improve The effect of improving machinability and strength

Active Publication Date: 2014-05-14
LANGFANG GAOCI NEW MATERIALS TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Among them, HTCC is an earlier developed technology. Since its process temperature needs to reach above 1300°C, the selection of electrodes used is limited, and the preparation cost is quite expensive.
Although the process temperature of LTCC is reduced to 850°C, the accuracy of the prepared circuit is relatively poor, and the thermal conductivity of the finished product is also low; the preparation method of DBC requires the formation of an alloy between copper foil and ceramics, and the calcining temperature needs to be strictly controlled at 1065-1085°C In the temperature range, because the preparation method of DBC has requirements on the thickness of the copper foil, generally not less than 150~300 microns, so the width-to-depth ratio of the wires of this type of ceramic circuit board is limited.
[0004] At present, the popular high thermal conductivity ceramic substrates on the market are generally prepared by DPC. The manufacture of DPC is carried out by repeated chemical plating on the surface of the ceramic plate for metal deposition, so that the surface produces conductors. However, the conductor on the surface of this ceramic plate is thin. , low peel strength, can not be machined

Method used

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Examples

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Effect test

preparation example Construction

[0030] In one embodiment of the present invention, a method for preparing the above-mentioned organic ceramic circuit board is provided, comprising the following steps: S1. mixing ceramic materials, coupling agents, and coupling agents to form organic ceramic materials; S2. mixing organic The ceramic material is poured into the mold for heating and solidification to form an organic ceramic board; S3. After coating vitrified agent on both side surfaces of the organic ceramic board, attaching a metal heat conducting plate, and fixing by heating to form an organic ceramic circuit board. The preparation method of the organic ceramic circuit board provided by the invention is simple, applicable and easy to produce in large quantities.

[0031] Preferably, in the step of heating and curing in step S2 of the above preparation method, the temperature is 80-150°C and the pressure is 20-25Mpa / cm 2Under certain conditions, press and solidify for 20-60 seconds to obtain the organic cerami...

Embodiment 1

[0036] The raw materials of the coupling agent: 10g of barium phenolic resin, 2g of epoxy resin E062, 0.5g of resorcinol, 8g of asbestos powder, and 100ml of methyl ethyl ketone.

[0037] Raw materials of the organic ceramic material: ceramic material (25g of aluminum oxide, 10g of silicon dioxide, 5g of aluminum nitride), 25g of coupling agent, and 0.5g of propylene trimethoxysilane.

[0038] The preparation method of organic ceramic circuit board:

[0039] S1. directly mix barium phenolic resin, E06 epoxy resin, resorcinol, asbestos powder, methyl ethyl ketone, ceramic material powder and coupling agent, and stir until powdery material is formed to form organic ceramic material powder;

[0040] S2. Pour the organic ceramic material powder into the mold at a temperature of 80°C and a pressure of 25Mpa / cm 2 Heating and curing under certain conditions, pressing and curing for 60s to form an organic ceramic plate;

[0041] S3. Coating vitrified agent on the two side surfaces o...

Embodiment 2

[0043] The raw materials of the coupling agent: 30g of barium phenolic resin, 10g of E06 epoxy resin, 5g of resorcinol, 15g of asbestos powder, and 80ml of methyl ethyl ketone.

[0044] Raw materials of the organic ceramic material: ceramic material (35g of aluminum oxide, 15g of silicon dioxide, 10g of aluminum nitride), 35g of coupling agent, and 1g of propylene trimethoxysilane.

[0045] The preparation method of organic ceramic circuit board:

[0046] S1. directly mix barium phenolic resin, E06 epoxy resin, resorcinol, asbestos powder, methyl ethyl ketone, ceramic material powder and coupling agent, and stir until powdery material is formed to form organic ceramic material powder;

[0047] S2. Pour the organic ceramic material powder into the mold at a temperature of 150°C and a pressure of 20Mpa / cm 2 Heating and curing under certain conditions, pressing and curing for 20s to form an organic ceramic plate;

[0048] S3. After coating the vitrified agent on the two side su...

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Abstract

The invention discloses a linking agent, an organic ceramic material, an organic ceramic circuit board and a preparation method thereof. The linking agent comprises, by weight, 10-30 parts of a barium phenolic resin, 2-10 parts of an E06 epoxy resin, 0.5-5 parts of meta-phenylenediamine, 8-15 parts of asbestos powder and a proper amount of methyl ethyl ketone. The organic ceramic material comprises, a linking agent accounting for 5-50% that of a total weight of the organic ceramic material, and a coupling agent accounting for 0.05-1% that of a total weight of the organic ceramic material. The linking agent, the organic ceramic material, the organic ceramic circuit board and the preparation method thereof are provided by the invention. The linking agent is formed by mixing the barium phenolic resin, the E06 epoxy resin, the meta-phenylenediamine powder and methyl ethyl ketone; the cross-linking agent can be bonded with the ceramic material in presence of the coupling agent, so that the ceramic material can be shaped at a relatively low temperature; the strength of a prepared organic ceramic wafer is improved; and heat conductivity coefficient is increased.

Description

technical field [0001] The invention relates to the field of ceramic materials, in particular to a coupling agent, an organic ceramic material, an organic ceramic circuit board and a preparation method thereof. Background technique [0002] With the gradual deepening of electronic technology in various application fields, the high integration of circuit boards has become an inevitable trend. Highly integrated modules require a good heat dissipation carrying system, while traditional circuit boards FR-4 and CEM-3 are in TC (thermal conductivity) The disadvantages in technology have become a bottleneck restricting the development of electronic technology. The LED industry, which has developed rapidly in recent years, has also put forward higher requirements for the TC index of its load-carrying circuit boards. In the field of high-power LED lighting, materials with good heat dissipation properties such as metal and ceramics are often used to prepare circuit substrates. At pre...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/634C04B35/10H05K1/03H05K3/00
Inventor 秦玉行王治虎赵绍春王庆杰
Owner LANGFANG GAOCI NEW MATERIALS TECH CO LTD
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