Preparation method and application of environment-friendly type shield tail sealing grease
An environment-friendly, shield-tail sealing technology, applied in the petroleum industry, lubricating compositions, etc., can solve problems such as poor pumpability and sealing and water-stop performance, uneven quality of sealing grease, and increased shield cost, etc., to achieve water resistance Strong pressure-tightness, excellent pumpability, and the effect of reducing clogging
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[0015] The preferred embodiment of the environment-friendly shield tail sealing grease of the present invention is:
[0016] Including the following components according to the mass ratio: lubricating oil 14-30%, oil plasticizer 7-22%, thickener 3-15%, grease 3-12%, natural degradable fiber 3-8% %, filling granular material 35-60%, color enhancer 1-3%, preservative 0.1-2%.
[0017] Described lubricating oil is the mixture of any one or more of the following: 32 # Mechanical hydraulic oil, 46 # Mechanical hydraulic oil, 68 # Mechanical hydraulic oil, anti-wear hydraulic oil.
[0018] The oil plasticizer is any one or a mixture of the following: chlorinated paraffin-42, chlorinated paraffin-52, chlorinated paraffin-70, DOP, DBP.
[0019] The thickener is any one or a mixture of the following: PIB, OCP, HSD, PMA, coumarone resin, agar, gum arabic, rosin and its derivatives, petroleum resin, and the like.
[0020] Described lubricating grease is the mixture of any one or more...
Embodiment l
[0032] First, the 200kg 32 # Add the mechanical hydraulic oil into the heating kettle, heat up to about 80°C while stirring, then add 30kg of thickener (m(PB2400):m(5T)=l:4), continue stirring and kneading for about 1~4h to mix evenly After that, cool down to 30~50°C. Afterwards, the lubricating oil and the thickening agent that will mix homogeneously are transferred in the grease kneader, and 100kg oil product plasticizer chlorinated paraffin-42,50kg 2 # Lithium base grease, 565kg of light calcium carbonate (5:3:2 in batches) were added to the oil kneader and kneaded until uniform under stirring conditions; finally, 35kg of degradable wood fiber, 5kg of preservatives and 15kg of anatase were added Type titanium dioxide, kneading and stirring at constant temperature for 1~3h, you can get the seal tail grease.
Embodiment 2
[0034] First, the 220kg 46 # Add the mechanical hydraulic oil into the heating kettle, heat up to about 80°C while stirring, then add 50kg of thickener (m(C5):m(rosin derivative)=2:3), continue stirring and kneading for about 1~4h After mixing evenly, cool down to 30~50°C. The lubricating oil that mixes homogeneously and the thickener are transferred in the grease kneader afterwards, and the oil product plasticizer chlorinated paraffin-52, 50kg complex soap base fat of 75kg, heavy calcium carbonate 550kg (add in batches 5: 3:2) Under the condition of stirring, add it into the oil kneader and knead until uniform; finally add 35kg of degradable wood fiber, 5kg of preservative and 15kg of anatase titanium dioxide, knead and stir at constant temperature for 1~3h, and then you can get the shield Tail seal grease.
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