Oil base drilling fluid wetting agent and application thereof
An oil-based drilling fluid and wetting agent technology, applied in the direction of drilling compositions, chemical instruments and methods, etc., can solve problems such as unsatisfactory wetting effect, drilling fluid sticking to drill pipe, insufficient temperature resistance, etc., to achieve Good economic and social benefits, little impact on rheology, and easy implementation
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Embodiment 1
[0027] Wetting performance test of wetting agents. In order to screen out a reasonable proportion of wetting agent components, this example prepared a variety of wetting agents and numbered them respectively; meanwhile, in order to simplify the test, vegetable oleic acid from soybean was used as an example for illustration. The method for evaluating the wetting performance of the wetting agent in this example refers to the content recorded in the description of Chinese patents: Publication No. CN102053045A, Application No. CN201010521882.8; Publication No. CN 102816556A, Application No. 201210335309.7.
[0028] Wetting agent preparation:
[0029] 1# wetting agent: the preparation of vegetable pine tar and vegetable oleic acid is 90-10 (weight percent), stirring and mixing for 30 minutes.
[0030] 2# Wetting agent: the preparation of vegetable pine tar and vegetable oleic acid is 85-15 (weight percent), stirring and mixing for 30 minutes.
[0031] 3# Wetting agent: the prepar...
Embodiment 2
[0049] In order to further illustrate the wetting performance of the oil-based drilling fluid wetting agent of the present invention, three commonly used wetting agents were selected to conduct a comparison test of wetting performance. The wetting agent used in this example is the 7# wetting agent prepared in Example 1, and the three comparative wetting agents are dodecyltrimethylammonium bromide, SPAN-80 and TWEEN-80. Test method with reference to embodiment 1. The wettability of lauryltrimethylammonium bromide, SPAN-80 and TWEEN-8 as wetting agent measured in this embodiment is respectively 68%, 75% and 73%, lower than 7# wetting The wetting rate (93%) of the wetting agent shows that the wetting performance of the 7# wetting agent prepared by the method of the present invention is better than three commonly used wetting agents, and can be used as a good substitute for commonly used wetting agents Oil-based drilling fluid.
Embodiment 3
[0051] In order to verify whether the optimal wetting agent formula (7# wetting agent) screened in Example 1 has a good wetting effect on various weighting materials, this example is based on Example 1 and Example 2 On the above, the wetting performance of 7# wetting agent was comprehensively evaluated. The weighting materials for the test (all particle sizes are 20 μm) are barite, iron ore powder, limestone powder, manganese tetroxide; the wetting agent for the test is 7# wetting agent, dodecyltrimethylammonium bromide, SPAN -80 and TWEEN-80. Test method with reference to embodiment 1. The measurement results of this embodiment are shown in Table 2.
[0052] Table 2 Wetting properties of several wetting agents on different weighted materials
[0053]
[0054] It can be seen from Table 2 that the wetting performance of 7# wetting agent on barite, iron ore powder, limestone powder and manganese tetroxide is better than that of commonly used wetting agents such as dodecylt...
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