Oil-based liquid-state fracturing fluid thickening agent, and preparation method thereof

A fracturing fluid thickener and liquefaction technology, which is applied in the field of liquefied thickener and the preparation of the above-mentioned liquefied thickener, can solve the problem of increasing the difficulty of fracturing fluid quality control, increasing the cleaning and processing cost of a liquid storage tank, increasing the problems such as manpower and material consumption, to achieve the effect of easy quality control, reduced manpower and material resources, and convenient preparation

Active Publication Date: 2014-07-09
北京爱普聚合科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] 1) The preparation of base liquid not only requires special equipment for mixing dry powder and water, but also easily produces "fish eyes" of different sizes and local agglomeration, which affects the quality of the base liquid;
[0009] 2) The construction flexibility is small. If the fracturing fluid volume is insufficient or the fracturing scale needs to be temporarily increased due to special reasons, it cannot be realized on site;
[0010] 3) There are many types of admixtures required, and the admixture steps are cumbersome, which increases the difficulty of controlling the quality of fracturing fluids;
[0011] 4) The hydration and swelling time of thickener dry powder is long (more than 10 minutes), which increases the consumption of manpower and material resources;
[0012] 5) There is a large amount of base fluid residue (10-30%) in the liquid storage tank after fracturing, which increases the cleaning and treatment costs of the liquid storage tank

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0062] Specifically, the preparation method of the oil-based liquid thickener of the present invention comprises the following steps:

[0063] The first step: the compounding of oil-based organic solvent

[0064]Keep the temperature in the kettle at 10-40°C, add fuel oil organic solvents (including but not limited to one or more of gasoline, diesel, kerosene) or mineral oil organic solvents (including but not limited to One or both of mineral oil and liquid paraffin) or silicone oil organic solvents (including but not limited to one or more of methyl silicone oil, ethyl silicone oil, methyl hydrogen silicone oil, phenyl silicone oil, methyl hydroxy silicone oil ) or vegetable oil organic solvent (including but not limited to one or more of rapeseed oil, corn oil, soybean oil, peanut oil, cottonseed oil), density regulator (dichloromethane, chloroform, carbon tetrachloride , one or more of chlorinated paraffin), performance modifier (one or more of nano-bentonite, polyamide wa...

Embodiment 1

[0074] Preparation and performance test of liquid thickener 1:

[0075] 1) Weigh 58g of gasoline and 57.5g of diesel oil in the kettle and keep stirring; add 21g of dichloromethane and 21.9g of chloroform and stir for 15min; add 6.6g of nano-bentonite and stir for 20min to obtain a compound oil-based organic solvent.

[0076] 2) Keep stirring, add 135 g of hydroxypropyl modified guar gum, and stir for 30 minutes to obtain liquefied thickener 1.

[0077] The product in this embodiment is an emulsion dispersion, and after testing, the density is 1.05g / cm 3 , the gelling time is 20s, and the viscosity of 1.2% liquefied thickener after dissolving is 45mPa.s.

Embodiment 2

[0079] Preparation and performance test of liquid thickener 2:

[0080] 1) Weigh 41g of liquid paraffin and 40g of methyl silicone oil in the kettle and keep stirring; add 7.2g of carbon tetrachloride and stir for 10min; add 0.9g of nano-bentonite and 0.9g of polyamide wax and stir for 25min to obtain the compounded Oil-based organic solvents.

[0081] 2) Keep stirring, add 60g of zwitterionic polyacrylamide and stir for 25min to obtain liquefied thickener 2.

[0082] The product in this embodiment is an emulsion dispersion, and after testing, the density is 1.10g / cm 3 , The gelling time is 20s, and the viscosity of 1.2% liquefied thickener after dissolving is 42mPa.s.

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Abstract

The invention discloses an oil-based liquid-state fracturing fluid thickening agent, and preparation method thereof. Density of the oil-based liquid-state fracturing fluid thickening agent ranges from 0.9 to 1.2g / cm<3>; gelling time is 20s or less; and viscosity of 1.2% of the oil-based liquid-state fracturing fluid thickening agent after dissolving is 30mPa.s or more. The invention also discloses a preparation method of the oil-based liquid-state fracturing fluid thickening agent.

Description

technical field [0001] The invention relates to an ultra-fast dissolving oil-based liquefied fracturing fluid thickener (hereinafter referred to as "liquefied thickener"). [0002] The present invention also relates to a method for preparing the above-mentioned liquefied thickener. Background technique [0003] Water-based fracturing fluid is an important technology for enhancing oil and gas recovery. In the water-based fracturing process, fine powder solid fracturing fluid thickeners are generally used, such as natural polymers, synthetic polymer thickener dry powder, etc. The dispersibility and hydration viscosity of the thickener determine the fracturing construction technology, fracturing quality and fracturing cost. [0004] The current fracturing construction technology is generally as follows: [0005] The first step is to prepare the base liquid, disperse the thickener dry powder in water, and fully swell within a certain period of time to form a base liquid with ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/64
CPCC09K8/68C09K8/882C09K8/90
Inventor 郑焰李树盛罗于建白小丹姚明龙乔磊
Owner 北京爱普聚合科技有限公司
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