Nano microcapsule material having self-repairing and wear-resisting functions and preparation method thereof
A nano-microcapsule and microcapsule finishing technology, which is applied in the direction of microcapsule preparation, microsphere preparation, textiles and papermaking, etc., can solve the problems of microfiber ineffectiveness, unsuitability for ultra-thin down jackets, and reduction of air permeability of fabrics. Good anti-drilling fleece, enhanced anti-drilling fleece performance, excellent perspiration and moisture permeable effect
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[0039] This example provides a nano-microcapsule material with self-healing and wear-resistant functions, which is prepared by the following steps:
[0040] (1) Chitosan modification: Add acetic acid solution into the reactor, add chitosan under nitrogen protection, heat to 65°C and stir until chitosan is completely dissolved, add ammonium persulfate, N,N′- Methyl bisacrylamide and acrylic acid, react at 65°C for 4 hours, stop the reaction, add ethanol, stir for 30 minutes, add alkali to adjust the pH to 7, filter, wash with water, soak in absolute ethanol for 24 hours, take it out, and dry it in vacuum. Obtain a white fluffy solid, and the mass ratio of acetic acid, chitosan, ammonium persulfate, N,N'-methylenebisacrylamide, acrylic acid and ethanol in the acetic acid solution is 3.5:15:1.5:0.3 in sequence :1:4;
[0041] (2) Introducing self-healing groups: Add the above-mentioned white fluffy solid, trithiocarbonate, ether, and azobisisobutyronitrile into the reactor at a ...
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