Green tea extract as well as preparation method and application thereof
A technology of green tea extract and green tea, applied in the field of tobacco spices
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Embodiment 1
[0020] Step 1: Add 1000g of green tea leaves to the ultrasonic extraction tank, add a mixed solvent with a weight ratio of ethanol: propylene glycol: water: malic acid = 30:10:58:2, the material-liquid ratio is 1:10, turn on the equipment, ultrasonic frequency At 25kHz, the temperature was kept at 75°C, the extraction time was 40 minutes, the operation was stopped, the extraction solution was poured out after a little cooling, filtered with a filter screen, and the extraction solution was collected; extract;
[0021] Step 2: Combine the two extracts, concentrate on a rotary evaporator, the concentration temperature is 70°C, and the vacuum degree is 0.005Mpa;
[0022] Step 3: dilute the obtained concentrate with 10 times of distilled water;
[0023] Step 4: Pass the diluted solution processed in Step 3 through the resin column at a flow rate of 1.5 BV / h. After the adsorption, the resin column was flushed with 5 L of distilled water at a flow rate of 1.5 BV / h. After rinsing, ...
Embodiment 2
[0026] Step 1: Add 1000g of green tea leaves into the ultrasonic extraction tank, add a mixed solvent with a weight ratio of ethanol: propylene glycol: water: malic acid = 20:20:50:3, the material-liquid ratio is 1:6, turn on the equipment, ultrasonic frequency At 20kHz, the temperature was kept at 80°C, the extraction time was 30 minutes, the operation was stopped, the extraction solution was poured out after a little cooling, filtered with a filter screen, and the extraction solution was collected; extract;
[0027] Step 2: Combine the two extracts, concentrate on a rotary evaporator, the concentration temperature is 65°C, and the vacuum degree is 0.01Mpa;
[0028] Step 3: dilute the obtained concentrate with 20 times of distilled water;
[0029] Step 4: Pass the diluted solution processed in Step 3 through the resin column at a flow rate of 1.5 BV / h. After the adsorption, the resin column was flushed with 5 L of distilled water at a flow rate of 1.5 BV / h. After rinsing, ...
Embodiment 3
[0033] Step 1: Add 1000g of green tea leaves to the ultrasonic extraction tank, add a mixed solvent with a weight ratio of ethanol: propylene glycol: water: malic acid = 30:20:60:4, the material-liquid ratio is 1:15, turn on the equipment, ultrasonic frequency At 200kHz, the temperature was kept at 60 °C, the extraction time was 60 minutes, the operation was stopped, the extraction solution was poured out after a little cooling, filtered with a filter screen, and the extraction solution was collected; extract;
[0034] Step 2: Combine the two extracts, concentrate on a rotary evaporator, the concentration temperature is 85°C, and the vacuum degree is 0.007Mpa;
[0035] Step 3: dilute the obtained concentrate with 15 times of distilled water;
[0036] Step 4: Pass the diluted solution processed in Step 3 through the resin column at a flow rate of 1.5 BV / h. After the adsorption, the resin column was flushed with 5 L of distilled water at a flow rate of 1.5 BV / h. After rinsing...
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