Preparation method of titanium oxide film and titanium oxide film
A titanium oxide film, titanium oxide technology, applied in the direction of titanium oxide/hydroxide, titanium dioxide, etc., can solve the problems of unsuitability for large-area and mass production of titanium oxide film, poor repeatability and uniformity, and long time consumption. Improve the utilization of sunlight, uniform aperture and density, smooth surface without cracks
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[0031] The invention provides a simple, fast and low-cost chemical preparation method of a novel nano-porous titanium oxide film structure material.
[0032] details as follows:
[0033] The first step, the preparation of titanium oxide precursor (such as figure 2 shown)
[0034] 1) Add diethanolamine dropwise to the stirring ethanol, the molar ratio is diethanolamine:ethanol=1:31.2, and stir at 40°C for 10-20 minutes to obtain solution A.
[0035] 2) Add butyl titanate to the above solution drop by drop, the molar ratio is butyl titanate:diethanolamine=1:1.62, and continue to stir at 40°C for 100-150 minutes to obtain solution B.
[0036] 3) Slowly add deionized water dropwise to the above system, the molar ratio is butyl titanate: water = 1:1.26, seal and stir for about 30-40 minutes to obtain light yellow transparent precursor solution C.
[0037] 4) Add a certain mass fraction of polyvinylpyrrolidone (molecular weight Mw=55000) to the light yellow transparent precursor...
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