Method for preparing pomegranate seed oil rich in vitamin E
A technology for pomegranate seed oil and vitamins, which is applied in the direction of producing fat, fat oil/fat production, etc., can solve the problems of not involving the extraction and protection of the antioxidant component vitamin E, not being able to well inhibit oxidation, and affecting the naturalness of oils and fats, etc. Widely used value, improving punicic acid content and oil yield, not easy to oxidize and deteriorate
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Embodiment 1
[0020] Example 1: 200g of pomegranate seeds were added with anti-oxidant protection agent: 1g of vitamin C, 1g of water-soluble tea polyphenols and 0.06g of vitamin E, after being crushed, sieved through a 10-mesh sieve, dried at 40°C for 4 hours, and added to the extraction kettle , adjust the extraction pressure to 28MPa, temperature to 55°C, flow rate to 15L / h, separation temperature to 50°C, separation pressure to 18MPa, and extraction for 3.5 hours. The separated carbon dioxide is liquefied and returned to the storage tank, and then recycled after being pressurized and heated. Isolate pomegranate seed oil 16g, its appearance is transparent and light in color. After analysis and detection, the content of punicic acid in the oil is 81%, the content of vitamin E is 200mg / 100g, the acid value is 2.5mgKOH / g, and the peroxide value is 0.08%.
Embodiment 2
[0021] Example 2: 200g of pomegranate seeds were added with anti-oxidant protection agent: 2g of vitamin C, 5g of fat-soluble tea polyphenols and 0.3g of vitamin E, after being crushed, sieved through a 40-mesh sieve, dried at 25°C for 6 hours, and then added to the extraction kettle , adjust the supercritical extraction separation parameters as in Example 1, and extract for 2.5 hours. 11g of pomegranate seed oil was isolated, and its appearance was transparent and light in color. After analysis and detection, the content of punicic acid in the oil is 83%, the content of vitamin E is 660mg / 100g, the acid value is 1.2 mgKOH / g, and the peroxide value is 0.02%.
Embodiment 3
[0022] Example 3: 200g of pomegranate seeds were added with anti-oxidant protection agent: 4g of vitamin C, 2g of fat-soluble tea polyphenols and 0.1g of vitamin E, after being crushed, sieved through a 20 mesh, dried at 85°C for 2 hours, and then added to the extraction kettle , adjust the extraction parameters: pressure 30MPa, temperature 45°C, flow rate 10L / h, separation temperature 40°C, separation pressure 10MPa, extraction for 3 hours. Isolate 28g of pomegranate seed oil, its appearance is transparent and light in color. After analysis and detection, the content of punicic acid in the oil is 85%, the content of vitamin E is 420mg / 100g, the acid value is 1.2mgKOH / g, and the peroxide value is 0.03%.
[0023] For the preparation method listed in the above-mentioned examples 1, 2, and 3, except the listed parameters for supercritical carbon dioxide extraction and separation, each parameter can be selected within the following ranges: extraction pressure 16-40MPa, extraction ...
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