Optical plastic protective coating and preparation method thereof

A technology for optical plastics and protective coatings, applied in the direction of coatings, etc., can solve the problems of low hardness and poor wear resistance of optical plastic coatings, and achieve the effects of high hardness and wear resistance, high light transmittance, and chemical structure improvement.

Inactive Publication Date: 2016-09-14
SHANGHAI INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] One of the objectives of the present invention is to provide an optical plastic protective coating in order to solve the above-mentioned technical problems such as low hardness and poor wear resistance of the optical plastic coating, which has high light transmittance and high hardness at the same time. features

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0034] An optical plastic protective coating, calculated in parts by weight, its composition and content are as follows:

[0035] Tetraethyl silicate 2 parts

[0036] 5 parts of phenyltrimethoxysilane

[0037] 1.5 parts of coupling agent

[0038] 4 parts distilled water

[0039] Curing agent 0.02 parts

[0040] Catalyst 0.02 part;

[0041] The coupling agent is γ-(2,3-epoxypropoxy)propyltrimethoxysilane;

[0042] Described solidifying agent is the hydrochloric acid aqueous solution that mass percent concentration is 38%;

[0043] The catalyst is dibutyltin dilaurate.

[0044] The preparation method of above-mentioned a kind of optical plastic protective coating, the steps are as follows:

[0045] Add 2 parts of ethyl orthosilicate, 5 parts of phenyltrimethoxysilane, 1.5 parts of coupling agent, 4 parts of distilled water, 0.02 parts of curing agent and 0.02 parts of catalyst into the container in sequence, stir and place at room temperature for 24 hours to obtain color...

Embodiment

[0052] An optical plastic protective coating, calculated in parts by weight, its composition and content are as follows:

[0053] Tetraethyl silicate 2 parts

[0054] 6.5 parts of phenyltrimethoxysilane

[0055] 2 parts of coupling agent

[0056] 3 parts distilled water

[0057] Curing agent 0.03 parts

[0058] Catalyst 0.04 part;

[0059] The coupling agent is γ-methacryloxypropyltrimethoxysilane;

[0060] Described curing agent is the sulfuric acid aqueous solution that mass percent concentration is 98%;

[0061] Described catalyst is stannous octoate.

[0062] The preparation method of above-mentioned a kind of optical plastic protective coating, the steps are as follows:

[0063] Add 2 parts of tetraethyl orthosilicate, 6.5 parts of phenyltrimethoxysilane, 2 parts of coupling agent, 3 parts of distilled water, 0.03 parts of curing agent and 0.04 parts of catalyst into the container in sequence, and leave it at room temperature for 24 hours after stirring to obtain ...

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Abstract

The invention discloses an optical plastic protective coating and a preparation method thereof. The optical plastic protective coating is calculated in parts by weight, that is, 2 parts of ethyl orthosilicate, 5-6.5 parts of phenyltrimethoxysilane, 1.5-2 parts of coupling agent, 3-4 parts of distilled water, 0.02 ~0.03 parts of curing agent and 0.02~0.04 parts of catalyst were added to the container in turn, stirred and left at room temperature for 24 hours, the obtained colorless and transparent liquid was coated on the optical plastic plate and dried at 80°C, and then placed on the optical plastic plate The resulting layer of coating is the optical plastic protective coating. The optical plastic protective coating has the characteristics of high light transmittance, high hardness, etc., and can be widely used in the field of optical plastic protection, and can also be used in the fields of coatings, inks, and the like.

Description

technical field [0001] The invention belongs to the technical field of polymer materials, and in particular relates to an optical plastic protective coating and a preparation method thereof. Background technique [0002] Compared with optical glass, optical plastic has many advantages such as light specific gravity, strong impact resistance, low cost, good light transmission, safety and reliability, etc., so it is widely used for making spectacle lenses, windshields on airplanes and cars, and cameras various lenses. However, optical plastics also have problems such as easy scratches and poor heat resistance. In order to overcome the above shortcomings, Zhang Chongzhao prepared a wear-resistant optical plastic protective optical plastic protective coating with a mixture of tetraalkoxysilane, trialkoxysilane, and dialkoxysilane through a catalytic reaction. The wear-resistant optical plastic protective coating has Certain hardness and wear resistance, but the siloxanes used ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D183/04C09D183/02C09D7/12C08J7/04
Inventor 张英强吴蓁陈丽顾亚峰崔边厅
Owner SHANGHAI INST OF TECH
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