Integrated treatment device and method for cleaning, reducing and drying electrolytic copper powder

A technology of electrolytic copper powder and processing equipment, which is applied in the field of electrolysis, can solve the problems of increased energy consumption, increased labor, leakage, leakage, etc., and achieves the effects of improving anti-oxidation performance, reducing labor, and improving quality

Active Publication Date: 2015-01-21
GRIPM ADVANCED MATERIALS CO LTD
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  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0002] In the production process of electrolytic copper powder, the copper powder produced by electrolysis needs to go through multiple processes such as cleaning, drying, reduction, drying, and grading to become a product. At present, most of them are independent unit processes. After washing with deionized water for multiple times, deacidification and saponification, it is sent to the centrifugal dryer in batches to remove most of the water, and then sent to the reduction furnace to continue drying until the water content is lower than 0.1%, and the copper powder is reduced under a hydrogen atmosphere. The oxygen contained in the copper powder will generally agglomerate after passing through the reduction furnace, and it needs to be crushed before continuing to be graded and batch-packed. In this way, the product needs to be transferred multiple times between multiple processes, and each process requires separate equipment. Not only It increases the amount of labor, increases energy consumption, and is prone to leakage and other phenomena during the transfer process.

Method used

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  • Integrated treatment device and method for cleaning, reducing and drying electrolytic copper powder

Examples

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Embodiment 1

[0027] Ordinary electrolytic copper powder is divided into two batches, one batch is processed by conventional process, washed seven times in powder washing machine, washed three times after saponification, dried by centrifugal dryer for 30 minutes, dried and reduced in reduction furnace at 480°C for 2 hours, and then After being crushed by a crusher and classified by an airflow classifier, the bulk density of the sieved -200 mesh copper powder is 1.78g / cm 3 , the oxygen content is 565ppm, and the water content is 0.04%. The other batch is washed 5 times in the electrolytic copper powder cleaning, reduction and drying integrated treatment device, soaked in hydrazine hydrate aqueous solution with a mass fraction of 3% for 30 minutes to reduce and deoxygenate the copper powder, and then use the mass fraction The surface anti-oxidation treatment was carried out with 0.3% BTA aqueous solution, and the immersion time was 40min. After draining the liquid, dehydrate it once by suctio...

Embodiment 2

[0029] Low bulk density electrolytic copper powder is divided into two batches, one batch is processed by conventional process, washed 10 times in powder washing machine, washed three times after saponification, dried by centrifugal dryer for 40min, dried and reduced in reduction furnace at 430℃ for 2.5 hours, and then crushed by a crusher and classified by an airflow classifier, the bulk density of the sieved -200 mesh copper powder is 1.18g / cm 3 , the oxygen content is 765ppm, and the water content is 0.07%. The other batch is washed 5 times in the electrolytic copper powder cleaning, reduction and drying integrated treatment device, soaked in hydrazine hydrate aqueous solution with a mass fraction of 3% for 40 minutes to reduce and deoxygenate the copper powder, and then use mass fraction The surface anti-oxidation treatment was carried out with 0.3% BTA aqueous solution, and the immersion time was 60min. After draining the liquid, dehydrate it once by suction filtration, a...

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Abstract

The invention belongs to the technical field of electrolysis and particularly relates to an integrated treatment device and a method for cleaning, reducing and drying electrolytic copper powder. According to the integrated treatment device for cleaning, reducing and drying electrolytic copper powder, a filtering layer is arranged inside a cavity of the integrated treatment device, and the cavity is divided into two parts, namely, an upper part and a lower part, by virtue of the filtering layer; a material charging opening, a liquid charging opening, a gas outlet and a material outlet are respectively formed in the upper part of the cavity; and a compressed gas inlet, a liquid outlet and a filtration-suction opening are respectively formed in the lower part of the cavity. By combining a plurality of treatment processes of electrolytic copper powder into the integrated treatment device, production devices can be decreased, the labor strength of operators is reduced, the energy consumption and the loss of the product are reduced and the yield and the quality of the product are improved.

Description

technical field [0001] The invention belongs to the technical field of electrolysis, and in particular relates to an integrated treatment device and method for cleaning, reducing and drying electrolytic copper powder. Background technique [0002] In the production process of electrolytic copper powder, the copper powder produced by electrolysis needs to go through multiple processes such as cleaning, drying, reduction, drying, and grading to become a product. At present, most of them are independent unit processes. Electrolytic copper powder is in the washing machine After washing with deionized water several times for deacidification and saponification, it is sent to the centrifugal dryer in batches to remove most of the water, and then sent to the reduction furnace to continue drying until the water content is lower than 0.1%, and the copper powder is removed by reduction under a hydrogen atmosphere The oxygen contained in the copper powder will generally agglomerate afte...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C25C7/06C25C5/02
Inventor 王跃发戴赫刘勇张景怀汪礼敏
Owner GRIPM ADVANCED MATERIALS CO LTD
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