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Medical metal ceramic material and preparation method thereof

A technology of cermet and ball-to-material ratio, applied in the field of medical materials

Active Publication Date: 2015-03-04
LONGJU CEMENTED CARBIDE SUZHOU CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003]Technical problem to be solved: The cermet materials used for artificial teeth need to have very good hardness, biocompatibility, bending strength, tensile strength, traditional The above-mentioned characteristics of some artificial tooth materials are relatively poor. The purpose of the present invention is to overcome the problems of poor biocompatibility, low hardness and low strength of some traditional artificial tooth materials. Therefore, the present invention proposes a medical metal with the above advantages. Ceramic material and its preparation method

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] (1) Take 15Kg of zirconia, 13Kg of titanium dioxide, 2Kg of nickel, 11Kg of magnesium silicate, 3Kg of cobalt, 4Kg of magnesium, 3Kg of tungsten silicide, 4Kg of aluminum carbide, and 8Kg of calcium metasilicate by weight, and carry out the above metal and ceramic materials respectively. Ball milling, the ball-to-material ratio is 40:1, the rotating speed of the ball mill is 450rpm, and the ball milling time is 3.5h;

[0039] (2) Pour the above ball-milled metal materials and ceramic materials into a high-speed mixer for high-speed mixing, and the speed of the high-speed mixer is 200rpm;

[0040] (3) Carry out vacuum high-temperature sintering of the cermet material uniformly mixed in step (2) in a high-temperature sintering furnace. The heating rate of the high-temperature sintering furnace is 25°C / min. Keep the temperature unchanged for 2.5 hours, then raise the temperature again at a rate of 30°C / min until the temperature in the high-temperature sintering furnace is ...

Embodiment 2

[0042] (1) Take zirconia 11Kg, titanium dioxide 17Kg, nickel 4Kg, magnesium silicate 6Kg, cobalt 7Kg, magnesium 2Kg, tungsten silicide 6Kg, aluminum carbide 2Kg, calcium metasilicate 4Kg respectively by weight, and carry out the above metal and ceramic materials respectively Ball milling, the ball-to-material ratio is 30:1, the rotating speed of the ball mill is 150rpm, and the ball milling time is 2h;

[0043] (2) Pour the above ball-milled metal materials and ceramic materials into a high-speed mixer for high-speed mixing, and the speed of the high-speed mixer is 100rpm;

[0044] (3) Carry out vacuum high-temperature sintering of the cermet material uniformly mixed in step (2) in a high-temperature sintering furnace. The heating rate of the high-temperature sintering furnace is 25°C / min. Keep the temperature unchanged for 2.5 hours, raise the temperature again, the heating rate is 30°C / min, the temperature in the high-temperature sintering furnace is raised to 1220°C, the si...

Embodiment 3

[0046] (1) Take 12Kg of zirconia, 16Kg of titanium dioxide, 3Kg of nickel, 9Kg of magnesium silicate, 4Kg of cobalt, 3Kg of magnesium, 5Kg of tungsten silicide, 4Kg of aluminum carbide, and 7Kg of calcium metasilicate by weight, and carry out the above metal and ceramic materials respectively. Ball milling, the ball-to-material ratio is 40:1, the rotating speed of the ball mill is 450rpm, and the ball milling time is 3.5h;

[0047] (2) Pour the above ball-milled metal materials and ceramic materials into a high-speed mixer for high-speed mixing, and the speed of the high-speed mixer is 200rpm;

[0048] (3) Carry out vacuum high-temperature sintering of the cermet material uniformly mixed in step (2) in a high-temperature sintering furnace. The heating rate of the high-temperature sintering furnace is 25°C / min. Keep the temperature unchanged for 2.5 hours, then raise the temperature again at a rate of 30°C / min until the temperature in the high-temperature sintering furnace is 9...

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Abstract

The invention belongs to the field of medical materials and discloses a medical metal ceramic material and a preparation method thereof. The medical metal ceramic material comprises 11-15 parts of zirconium oxide, 13-17 parts of titanium dioxide, 2-4 parts of nickel, 6-11 parts of magnesium silicate, 3-7 parts of cobalt, 2-4 parts of magnesium, 3-6 parts of tungsten silicide,2-4 parts of aluminum carbonate and 4-8 parts of calcium metasilicate. The preparation method comprises the following steps: (1) respectively ball-milling the metals and a ceramic material; (2) pouring into a high-speed mixture and mixing at a high speed; and (3) sintering in vacuum at a high temperature, firstly heating the inside of a high-temperature sintering furnace to the temperature of 725-755 DEG C, heating the inside of the high-temperature sintering furnace again to the temperature of 980-1220 DEG C, sintering for 2.5-3.5 hours, and cooling the metal ceramic material inside the high-temperature sintering furnace to room temperature to obtain the medical metal ceramic material.

Description

technical field [0001] The invention belongs to the field of medical materials, and relates to a cermet material and a preparation method thereof, in particular to a medical cermet material and a preparation method thereof. Background technique [0002] Cermet material is a material formed by high temperature treatment process, so it has the dual advantages of metal and ceramics: (1) Because it is sintered at high temperature, its structure includes ionic bonds or covalent bonds with strong bonds , so it has good mechanical strength, hardness, high compressive strength, and is extremely stable; it is difficult to dissolve in the body, not easy to oxidize, not easy to corrode and deteriorate, good thermal stability, easy to heat and disinfect, wear-resistant, has certain lubricating properties, and is not easy to produce fatigue phenomenon , and has good affinity with human tissue, and almost no repulsion with human tissue can be seen, so it can meet the requirements of impla...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C29/00C22C1/05
CPCC22C1/05C22C29/00
Inventor 金仲恩全春兰张帆
Owner LONGJU CEMENTED CARBIDE SUZHOU CO LTD
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