Medical metal ceramic material and preparation method thereof
A technology of cermet and ball-to-material ratio, applied in the field of medical materials
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Embodiment 1
[0038] (1) Take 15Kg of zirconia, 13Kg of titanium dioxide, 2Kg of nickel, 11Kg of magnesium silicate, 3Kg of cobalt, 4Kg of magnesium, 3Kg of tungsten silicide, 4Kg of aluminum carbide, and 8Kg of calcium metasilicate by weight, and carry out the above metal and ceramic materials respectively. Ball milling, the ball-to-material ratio is 40:1, the rotating speed of the ball mill is 450rpm, and the ball milling time is 3.5h;
[0039] (2) Pour the above ball-milled metal materials and ceramic materials into a high-speed mixer for high-speed mixing, and the speed of the high-speed mixer is 200rpm;
[0040] (3) Carry out vacuum high-temperature sintering of the cermet material uniformly mixed in step (2) in a high-temperature sintering furnace. The heating rate of the high-temperature sintering furnace is 25°C / min. Keep the temperature unchanged for 2.5 hours, then raise the temperature again at a rate of 30°C / min until the temperature in the high-temperature sintering furnace is ...
Embodiment 2
[0042] (1) Take zirconia 11Kg, titanium dioxide 17Kg, nickel 4Kg, magnesium silicate 6Kg, cobalt 7Kg, magnesium 2Kg, tungsten silicide 6Kg, aluminum carbide 2Kg, calcium metasilicate 4Kg respectively by weight, and carry out the above metal and ceramic materials respectively Ball milling, the ball-to-material ratio is 30:1, the rotating speed of the ball mill is 150rpm, and the ball milling time is 2h;
[0043] (2) Pour the above ball-milled metal materials and ceramic materials into a high-speed mixer for high-speed mixing, and the speed of the high-speed mixer is 100rpm;
[0044] (3) Carry out vacuum high-temperature sintering of the cermet material uniformly mixed in step (2) in a high-temperature sintering furnace. The heating rate of the high-temperature sintering furnace is 25°C / min. Keep the temperature unchanged for 2.5 hours, raise the temperature again, the heating rate is 30°C / min, the temperature in the high-temperature sintering furnace is raised to 1220°C, the si...
Embodiment 3
[0046] (1) Take 12Kg of zirconia, 16Kg of titanium dioxide, 3Kg of nickel, 9Kg of magnesium silicate, 4Kg of cobalt, 3Kg of magnesium, 5Kg of tungsten silicide, 4Kg of aluminum carbide, and 7Kg of calcium metasilicate by weight, and carry out the above metal and ceramic materials respectively. Ball milling, the ball-to-material ratio is 40:1, the rotating speed of the ball mill is 450rpm, and the ball milling time is 3.5h;
[0047] (2) Pour the above ball-milled metal materials and ceramic materials into a high-speed mixer for high-speed mixing, and the speed of the high-speed mixer is 200rpm;
[0048] (3) Carry out vacuum high-temperature sintering of the cermet material uniformly mixed in step (2) in a high-temperature sintering furnace. The heating rate of the high-temperature sintering furnace is 25°C / min. Keep the temperature unchanged for 2.5 hours, then raise the temperature again at a rate of 30°C / min until the temperature in the high-temperature sintering furnace is 9...
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