Method for preparing tar, coal gas and semi-coke by virtue of pyrolysis of bituminous coal

A semi-coke and tar technology, used in coke ovens, petroleum industry, special forms of dry distillation, etc., can solve the problems of easy blockage of the follow-up system, complicated process flow, and large amount of entrained dust, so as to improve the utilization rate of raw materials and reduce the dust content. volume, the effect of increasing gas production

Inactive Publication Date: 2015-04-22
CHENGDU HOT NEW ENERGY TECH
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Problems solved by technology

However, the technological process is complicated, and there are many stages. During the operation, it is necessary to take into account the set temperature, pressure, fluidization state and semi-coke discharge of each stage of the fluidized pyrolysis furnace, which makes the control difficult.
Due to the large amount of dust entrained in the fluidized bed gas, the follow-up system is easy to block, and the tar contains a lot of fine-grained semi-coke, which needs to be removed
[0005] The purpose of the present invention is to provide a coal pyrolysis upgrading method to solve the problems of low heat utilization rate, low oil and gas yield, and large amount of dust in the prior art.

Method used

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  • Method for preparing tar, coal gas and semi-coke by virtue of pyrolysis of bituminous coal
  • Method for preparing tar, coal gas and semi-coke by virtue of pyrolysis of bituminous coal
  • Method for preparing tar, coal gas and semi-coke by virtue of pyrolysis of bituminous coal

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Embodiment 1

[0038] The raw material coal of embodiment is long-flame coal, and raw material analysis data is as shown in table 1:

[0039] Table 1 raw material analysis table

[0040]

[0041] a. Send the raw coal with particle size ≤ 30mm to the screening and drying section. The raw coal is heated and dried by hot flue gas to a moisture content of 4%, and the raw coal is screened by wind force with hot flue gas. The coal powder with a particle size below 1mm is heated by hot flue gas The gas is sent to the pulverized coal separator for separation.

[0042] b. The sieved and dried raw coal with a particle size greater than 1mm is sent to the low-temperature pyrolysis section. The raw coal is heated to about 560°C by an external heat source, and the raw coal is pyrolyzed to generate hot semi-coke solid products, a large amount of tar steam and a small amount of gas ; The time of low temperature pyrolysis is 38 minutes.

[0043]c. The hot semi-coke solid product generated in the low-te...

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Abstract

The invention discloses a method for preparing tar, coal gas and semi-coke by virtue of pyrolysis of low-rank coal. The method comprises the following steps of processing pulverized raw material coal as in a three-stage manner, namely, a screening drying stage as the first stage, a low-temperature pyrolysis stage as the second stage and a medium-temperature pyrolysis stage as the third stage, wherein in the first stage, most moisture in the raw material coal is removed, the pulverized coal having the size of below 1mm is screened by wind power and used as a combustion raw material of a three-waste furnace for providing a heat source for a system, dust having the size of below 50 microns in the system is almost removed so that the pre-dust removal effect is achieved and the content of the dust in the end product coal tar is greatly reduced; during the second stage, the reaction temperature is controlled to be about 550-570 DEG C, and thus the highest tar yield is ensured; during the third stage, the reaction temperature is controlled to be about 690-710 DEG C the yield of the coal gas is increased. The products have the advantages of good quality, high yield, energy conservation and environment friendliness and the method has good economic and social benefits and is worthy in popularization and application.

Description

technical field [0001] The invention belongs to the field of coal chemical industry, and relates to a coal pyrolysis upgrading method, in particular to a method for preparing semi-coke, tar and gas by pyrolysis of low-rank coal. Background technique [0002] Low-metamorphic bituminous coal has the characteristics of high moisture, high volatile matter, and low calorific value. It has abundant reserves, but its thermal efficiency of direct combustion for power generation is low. How to efficiently utilize low-rank coal resources has gradually become the focus of development and research. Pyrolysis (dry distillation) technology is a commonly used coal processing technology. Since the last century, experts and scholars at home and abroad have developed various processes for coal pyrolysis technology. [0003] The main representative of foreign vertical internal heat retort furnace is the Lurgi-Spierges (L-S) low temperature retort furnace, which was developed by Lurqi GmbH in G...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10B53/04C10B57/02C10B57/10C10B57/00
CPCY02P20/133C10B53/04C10B57/00C10B57/02C10B57/10
Inventor 肖峰李敬德杜万斗白立强叶永强郎文莉
Owner CHENGDU HOT NEW ENERGY TECH
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