The application discloses a kind of methods for
hydrothermal treatment regulation and control of phenolic hydroxyl in
coal, it is related to the field of
coal processing and utilization, the method comprises the following steps: S1,
vacuum drying treatment is carried out to
coal sample, and pretreated coal sample is obtained;S2, the pretreated coal sample is mixed with reaction medium and sealed, and a mixture is obtained;S3, the mixture is heated for
hydrothermal reaction, and after heat preservation and pressure preservation, cooling, pressure relief, the
solid product is taken out and washed to neutral,
vacuum drying treatment is carried out, and the regulated and controlled coal sample is obtained.The process flow of the application is simple, the requirement for equipment is low, easy to enlarge implementation, only needs conventional high-pressure reaction kettle, without special
atmosphere protection or complex separation device, can be directly applied on existing
coal chemical industry hydrothermal treatment equipment, has better industrial adaptability, and then can be popularized to different coal kinds and scale
production line, provides universal technical scheme for directional regulation and control of functional groups in coal, thereby powerfully promotes the process of fine
processing and utilization of coal.