Method for preparing filtering absorbing material used for water treatment
A technology of water treatment and drying treatment, applied in water/sewage treatment, water/sludge/sewage treatment, filtration and separation, etc., can solve the problems of large amount of adsorbent, small specific surface area, frequent replacement, etc., and achieve simple preparation method , The effect of cheap and easy-to-obtain raw materials
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[0008] In the preparation method of the present invention, when selecting the raw material of the filter adsorbent, a suitable raw material should be selected according to the use requirements and parameters of the filter adsorbent, and then among a variety of suitable raw materials, a kind of filter adsorbent with the lowest cost should be selected and used raw materials. When calculating the production cost of the filter adsorbent, in addition to the price and freight of the raw material, the composition, activity of the raw material and the yield of the prepared filter adsorbent should also be compared. Generally, coal with a low degree of metamorphism has high volatile content, low ash content, and high activity. At a lower activation temperature, a filter adsorbent with a higher specific surface area can be obtained, but the yield of the filter adsorbate is low; Coal has low volatile content, high ash content, and poor reactivity. Under the same activation temperature or ...
Embodiment 1
[0022] Preparation of filter adsorbent
[0023] The raw material for preparing the filter adsorbent is long-flame coal (Shenmu bituminous coal). Long-flame coal (Shenmu bituminous coal) has high volatile content, low ash content, and high reactivity. Therefore, a filter adsorbent with a high specific surface area can be obtained at a low activation temperature, but the yield of filter adsorbate is low.
[0024] The long-flame coal (Shenmu bituminous coal) is crushed by crushing equipment, and then screened by screening equipment to make raw materials with a particle size of <10mm. The processed raw materials are transported to drying and carbonization equipment for drying and carbonization. The initial drying temperature is 120°C, and the temperature is raised at a rate of 4°C / min, and the drying temperature is 150-400°C. After the raw material is dried, continue to heat up to 580°C at a rate of 6-8°C / min, and then keep the temperature for 50 minutes to dry-distill and carbo...
Embodiment 2
[0038] (Jincheng) anthracite is used as the raw material for preparing the filter adsorbent. (Jincheng) anthracite has low volatile content, high ash content, and low reactivity. Therefore, compared with long-flame coal (Shenmu bituminous coal), the activation reaction temperature is higher, and the specific surface area of the filtered adsorbent is lower, but the yield of the filtered adsorbent is higher. Its operation steps are with embodiment 1.
[0039] The main parameters of the filter adsorbent prepared by embodiment 2:
[0040] Methylene blue: 32mg / g
[0041] Ash: 15%
[0042] Filling density 200g / l
[0043] Iodine value: 260mg / g
[0044] Specific surface area: 210m 2 / g
[0045] Activation reaction temperature: 950°C
[0046] Activation time: 60min
[0047] Filter adsorption material yield: 500kg / t. Coal
[0048] Chemical oxygen demand (CODcr) adsorption capacity: <1,600mg / g
[0049] Table 3 is the experimental record of using the filter adsorbent prepared in...
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