Formula of environment-friendly particle hot-melt type pressure-sensitive adhesive and preparation method for adhesive

A green, environmentally friendly, hot-melt technology, applied in the direction of adhesives, adhesive types, mineral oil hydrocarbon copolymer adhesives, etc., can solve the problems of adding toxic reagents and raw materials that cannot be recycled, so as to reduce labor and improve economy Benefits and industrial production prospects, the effect of increasing production

Inactive Publication Date: 2015-05-13
湖南鑫湘环保胶业科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Aiming at the defect that the raw materials of hot-melt pressure-sensitive adhesives in the prior art are mostly petrochemical products, which cannot meet the needs of sustainable development of human beings, the present invention provides a formula of green and environmentally friendly granular hot-melt pressure-sensitive adhesives. The pressure-sensitive adhesive is obtained by mixing renewable natural synthetic epoxy vegetable oil with synthetic rubber, resi...

Method used

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Examples

Experimental program
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Effect test

preparation example Construction

[0022] The preparation method of the above-mentioned green environmental protection granular hot-melt pressure-sensitive adhesive comprises the following steps: heating the kneader to 140-160°C, adding 30-40 parts of softener and 0.5-1 part of antioxidant, and then adding 5 - After 8 parts of polystyrene-polyisoprene-polystyrene block copolymer, 5-8 parts of styrene-ethylene / butadiene-styrene copolymer, 5-10 parts of ethylene / vinyl acetate copolymer resin Heat up and knead to 180-190°C, add 53-68 parts of tackifier and 2-5 parts of polyisobutylene after 20-25 minutes, cool down, knead and vacuumize to 120°C, filter out the glue, cool, cut into pellets, and cool and air-dry , Automatic measurement, weighing and packaging to obtain green environmental protection granular hot-melt pressure-sensitive adhesive. Among them, when the glue is discharged, the special anti-sticking polymer of the glue-out die head is used to automatically wrap the granular glue inside to play an anti-st...

Embodiment 1

[0026] A kind of formula of green environmental protection granular hot-melt pressure-sensitive adhesive, this hot-melt adhesive comprises following components: polystyrene-polyisoprene-polystyrene block copolymer 5kg, styrene-ethylene / butanediene ethylene-styrene copolymer 5kg, ethylene / vinyl acetate copolymer resin 5kg, softener 30kg (including synthetic epoxy vegetable oil 25kg, rubber softening oil PW-32 5kg), antioxidant 0.5kg (of which four (β-(3, 5-di-tert-butyl (4-hydroxyphenyl) propionate) pentaerythritol ester 0.25kg, β-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate n-octadecyl ester 0.25kg), 53kg of tackifier (of which petroleum resin is obtained by mixing 15kg of C5-100L and 18kg of Sn-400, rosin modified resin is 20kg of K-100), polyisobutylene 2kg.

[0027] The preparation method of the above-mentioned green environmental protection granular hot-melt pressure-sensitive adhesive comprises the following steps: heating the kneader to 140°C, adding 30kg of softener a...

Embodiment 2

[0029] A kind of formula of green environmental protection granular hot-melt pressure-sensitive adhesive, this hot-melt adhesive comprises following components: polystyrene-polyisoprene-polystyrene block copolymer 8kg, styrene-ethylene / butanediene ethylene-styrene copolymer 8kg, ethylene / vinyl acetate copolymer resin 10kg, softener 40kg (including synthetic epoxy vegetable oil 30kg, rubber softening oil PW-32 10kg), antioxidant 1kg (of which four (β-(3,5 -Di-tert-butyl (4-hydroxyphenyl) propionate) pentaerythritol ester 0.4kg, β-(3,5-di-tert-butyl-4-hydroxyphenyl) propionate n-octadecyl ester 0.6kg), Adhesive 68kg (including petroleum resin 20kgC5-100L mixed with 23kgSn-400, rosin modified resin K-100 25kg), polyisobutylene 5kg.

[0030] The preparation method of the above-mentioned green environmental protection granular hot-melt pressure-sensitive adhesive comprises the following steps: heating the kneader to 160°C, adding 40kg of softener and 1kg of antioxidant, and then se...

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Abstract

The invention discloses a formula of an environment-friendly particle hot-melt type pressure-sensitive adhesive. The hot metal adhesive is prepared from the following components in parts by weight: 5-8 parts of polystyrene-polyisoprene-polystyrene segmented copolymer, 5-8 parts of styrene-ethylene/butadiene-styrol copolymer, 5-10 parts of ethylene/vinyl acetate copolymerized resin, 30-40 parts of a softener, 0.5-1 parts of an antioxidant, 53-68 parts of a thickening agent, and 2-5 parts of polyisobutene. The invention further provides a method for preparing the environment-friendly particle hot-melt type pressure-sensitive adhesive. According to the formula and the preparation method disclosed by the invention, the particle hot-melt type pressure-sensitive adhesive is prepared by mixing a reproducible naturally synthesized epoxy plant oil as a raw material, synthetic rubber and resin as well as rubber oil, so that the problems that in the current pressure-sensitive adhesive industry, most of the raw materials cannot be recycled and toxic reagents are added in the process can be solved; and the product is environment-friendly, safe and harmless, easy to adhere, low in possibility to remove and non-destructive while being peeled off, and can be widely applied to the fields of sanitary material, medical treatment and the like.

Description

technical field [0001] The invention relates to the field of hot-melt adhesives, in particular to a formulation and a preparation method of a green environmental protection granular hot-melt pressure-sensitive adhesive. Background technique [0002] Most of the solvents added in the traditional hot melt adhesive production process at home and abroad are toxic reagents, which are harmful to the environment and human body. Hot-melt pressure-sensitive adhesives are solvent-free, more conducive to environmental protection and safe production, high production efficiency, and relatively low production costs, so countries around the world are vigorously developing hot-melt pressure-sensitive adhesives. Hot-melt pressure-sensitive adhesives are widely used in packaging and encapsulation of various products, medical adhesives, and disposable sanitary products. The needs of sustainable development of human beings; and the existing production process requires a relatively large site, ...

Claims

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Application Information

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IPC IPC(8): C09J157/02C09J193/04C09J153/02C09J123/08C09J123/20C09J11/06
Inventor 颜杰
Owner 湖南鑫湘环保胶业科技有限公司
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