Nano-chitosan composite material and nano-coated particle products
A nano-chitosan, composite material technology, applied in soil conditioning materials, organic fertilizers, fertilizer mixtures, etc., can solve problems such as soil pollution, long decomposition time, plant death, etc., to ensure survival and growth, good water retention, inhibiting The effect of water and fertilizer loss
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Embodiment 1
[0038] Embodiment 1 Preparation of nano-chitosan composite material and nano-coated particle products
[0039] In the present embodiment, PLA (polylactic acid), chitosan and hydroxypropyl methylcellulose are used as main raw materials, wherein, polylactic acid 2g, hydroxypropylmethylcellulose 10g, chitosan 5g, vinyl ketone 10g of quasi-polymer, 0.5g of oxygen release agent, 0.1g of dispersant, 0.1g of nano particle additive; 0.5g of curing agent, 200ml of distilled water. Concrete process steps are as follows:
[0040] (1) At normal temperature and pressure, dissolve 2g of polylactic acid in 20ml of dichloromethane to prepare a PLA organic solution with a mass percentage of 7.9%, then heat it to 50°C under normal pressure, and add 10g of hydroxypropylmethyl Cellulose, mixed evenly to form a PLA-hydroxypropyl methylcellulose mixed solution, under the conditions of normal pressure, 70°C, and nitrogen protection, a polymerization reaction occurred to obtain a jelly, and the reac...
Embodiment 2
[0046] Example 2 Preparation of nano-chitosan composite material and nano-coated particle products
[0047] In this embodiment, PLA (polylactic acid), chitosan and hydroxypropyl methylcellulose are used as main raw materials, wherein, polylactic acid 4g, hydroxypropylmethylcellulose 20g, chitosan 10g, vinyl ketone 15g of quasi-polymer, 1g of oxygen release agent, 0.16g of dispersant, 0.12g of nano particle additive; 0.8g of curing agent, 200ml of distilled water. Concrete process steps are as follows:
[0048] (1) Preparation of polymer composite solution:
[0049] Dissolve 4g of polylactic acid in 20ml of organic solvent methylene chloride under normal temperature and pressure to prepare a PLA organic solution with a mass percentage of 13.3%. base cellulose to form a PLA-hydroxypropyl methylcellulose mixed solution. Under normal pressure, 70° C., under the environment of nitrogen protection, a polymerization reaction occurs under the action of an initiator to obtain a jell...
Embodiment 3
[0050] Example 3 Preparation of nano-chitosan composite material and nano-coated particle products
[0051] In this embodiment, PLA (polylactic acid), chitosan and hydroxypropyl methylcellulose are used as main raw materials, wherein, polylactic acid 6g, hydroxypropylmethylcellulose 30g, chitosan 15g, vinyl ketone 20g of quasi-polymer, 1.5g of oxygen release agent, 0.18g of dispersant, 0.14g of nano particle additive; 1g of curing agent, 200ml of distilled water. Concrete process steps are as follows:
[0052] (1) Preparation of polymer composite solution:
[0053] Dissolve 6g of polylactic acid in 20ml of organic solvent dichloromethane under normal temperature and pressure, and prepare a PLA organic solution with a mass percentage of 18.7%. base cellulose to form a PLA-hydroxypropyl methylcellulose mixed solution. Under normal pressure, 70° C., under the environment of nitrogen protection, a polymerization reaction occurs under the action of an initiator to obtain a jelly...
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