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Aromatic and antibacterial tanning agent based on plane grass extract and preparation method thereof

A technology of aircraft grass and extracts, which is applied in the field of functional leather chemical materials and its preparation, can solve the problem of no resource utilization, limited ability to combine retanning agents and leather collagen fibers, and obstacles to retanning agents and leather collagen fibers. Combination and other issues

Inactive Publication Date: 2017-02-15
YUNNAN NORMAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the problem is that when entering the retanning process, the collagen fibers in the leather have been combined with the tanning agent and finalized (Shi Kaiqi, Yin Weigang, Li Ya, etc. Research on the fixation of animal tissues by tanning. Leather Science and Engineering , 2011,21(6):39-42.), which makes ① the tanning agent filled or combined inside the collagen fibers and in the fiber gaps will hinder the combination of the retanning agent and leather collagen fibers; ② the retanning agent It can also be combined with tanning agents to form macromolecules, which is not conducive to its penetration into the collagen fibers, which will eventually lead to limited binding ability between the retanning agent and skin collagen fibers, and it is mainly distributed in the collagen fiber gap
It is difficult to control and treat the aircraft grass after it invades, and there is no mature resource utilization method

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] In this embodiment, the aromatic antibacterial tanning agent is prepared according to the following steps, using aircraft grass produced in Chenggong District, Kunming City, Yunnan Province as raw material:

[0026] Collect the above-ground parts of the adult plants of Airplane Grass, dry and remove impurities, and crush them with a crusher. Screen out the aircraft grass material with a length of 2-10 mm and pack it into 10 m 3 In the tank, 6 tank groups are used for continuous countercurrent leaching, and water is added to the tank according to the solid-liquid mass ratio of 1:5. The extraction time of plane grass in each tank is 2 hours, and the total extraction cycle is 12 hours. The pressure of the tail tank is 0.3-0.35MPa, and the extraction temperatures are 80°C, 85°C, 90°C, 95°C, 100°C, and 110°C. The extract is transported into an evaporator for concentration to obtain a concentrated solution of crude tannin extract with a solid mass percentage of 25.0%.

[00...

Embodiment 2

[0031] In this embodiment, the aromatic antibacterial tanning agent is prepared according to the following steps, using the aircraft grass produced in Wuming County, Nanning City, Guangxi Province as raw material:

[0032] Collect the above-ground parts of the adult plants of Airplane Grass, dry and remove impurities, and crush them with a crusher. Screen out the aircraft grass material with a length of 10-20mm and pack it into 10m 3 In the tank, 4 tank groups are used for continuous countercurrent extraction, and water is added to the tank according to the solid-liquid mass ratio of 1:6. The extraction time of plane grass in each tank is 2.5 hours, and the total extraction cycle is 10 hours. The pressure of the tail tank is 0.35-0.4MPa, and the extraction temperatures are 80°C, 90°C, 100°C, and 110°C. The extract is transported into an evaporator for concentration to obtain a crude extract concentrate with a solid mass percentage of 28.5%.

[0033] Screen out the aircraft g...

Embodiment 3

[0037] In this embodiment, the aromatic antibacterial tanning agent is prepared according to the following steps, using the aircraft grass produced in Xinhui District, Jiangmen City, Guangdong Province as raw material:

[0038] Collect the above-ground parts of the adult plants of Airplane Grass, dry and remove impurities, and crush them with a crusher. Screen out the aircraft grass material with a length of 2-10 mm and pack it into 10 m 3 In the tank, 4 tank groups are used for continuous countercurrent leaching, and water is added to the tank according to the solid-liquid mass ratio of 1:7. The extraction time of plane grass in each tank is 2.5 hours, and the total extraction cycle is 10 hours. The pressure of the tail tank is 0.35-0.4MPa, and the extraction temperatures are 80°C, 90°C, 100°C, and 110°C. The extract is transported into the evaporator for concentration to obtain a crude extract concentrate with a solid mass percentage of 30.0%.

[0039] Screen out the aircr...

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Abstract

The present invention discloses an aromatic antibacterial tanning agent based on a fragrant eupatorium herb extract, and a preparation method thereof, wherein a fragrant eupatorium herb water extract, one or a plurality of fragrant eupatorium herb solvent extracts, and one or a plurality of aromatic agents are compounded to obtain the aromatic antibacterial tanning agent. According to the present invention, after single tanning through the aromatic antibacterial tanning agent of the present invention, the leather shrinkage temperature can be close to 90 DEG C, the aroma retaining time of the leather is more than 180 days, and the good inhibition effects are provided for bacteria adopting staphylococcus aureus as the representative, yeast adopting Cryptococcus albidus as the representative, mould adopting Aspergillus niger as the representative, and other leather bacteria; the fragrant eupatorium herb being the harmful invasive plant is subjected to resource utilization, such that the fragrant eupatorium herb can become the treasure, and the significant economic benefits can be generated so as to achieve the two purposes; and the aromatic antibacterial tanning agent of the present invention has three functions of tanning, aromatic property and antibacterial property, and can provide a new selection for the multi-functional leather chemical industry material.

Description

technical field [0001] The invention belongs to the technical field of functional leather chemical materials and preparation methods thereof, and in particular relates to an aromatic and antibacterial tanning agent based on extracts of japonica grass and a preparation method thereof. Background technique [0002] Leather and its products have excellent hygienic properties such as air permeability and water vapor permeability, and have been more and more widely used in people's daily life, including clothing, bags, furniture, decorations, etc. With the continuous development of human society, people's requirements for leather and its products are also increasing. For example, in addition to the basic functions of conventional leather clothing, durable luggage and furniture, requirements such as comfort, safety, pleasure, and individuality have also been put forward, which also calls for the birth and vigorous development of functional leather chemical materials. For example, ...

Claims

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Application Information

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IPC IPC(8): C14C3/12
CPCC14C3/12
Inventor 龚英陈继平陆俊余刘光娇
Owner YUNNAN NORMAL UNIV