Aromatic and antibacterial tanning agent based on plane grass extract and preparation method thereof
A technology of aircraft grass and extracts, which is applied in the field of functional leather chemical materials and its preparation, can solve the problem of no resource utilization, limited ability to combine retanning agents and leather collagen fibers, and obstacles to retanning agents and leather collagen fibers. Combination and other issues
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Embodiment 1
[0025] In this embodiment, the aromatic antibacterial tanning agent is prepared according to the following steps, using aircraft grass produced in Chenggong District, Kunming City, Yunnan Province as raw material:
[0026] Collect the above-ground parts of the adult plants of Airplane Grass, dry and remove impurities, and crush them with a crusher. Screen out the aircraft grass material with a length of 2-10 mm and pack it into 10 m 3 In the tank, 6 tank groups are used for continuous countercurrent leaching, and water is added to the tank according to the solid-liquid mass ratio of 1:5. The extraction time of plane grass in each tank is 2 hours, and the total extraction cycle is 12 hours. The pressure of the tail tank is 0.3-0.35MPa, and the extraction temperatures are 80°C, 85°C, 90°C, 95°C, 100°C, and 110°C. The extract is transported into an evaporator for concentration to obtain a concentrated solution of crude tannin extract with a solid mass percentage of 25.0%.
[00...
Embodiment 2
[0031] In this embodiment, the aromatic antibacterial tanning agent is prepared according to the following steps, using the aircraft grass produced in Wuming County, Nanning City, Guangxi Province as raw material:
[0032] Collect the above-ground parts of the adult plants of Airplane Grass, dry and remove impurities, and crush them with a crusher. Screen out the aircraft grass material with a length of 10-20mm and pack it into 10m 3 In the tank, 4 tank groups are used for continuous countercurrent extraction, and water is added to the tank according to the solid-liquid mass ratio of 1:6. The extraction time of plane grass in each tank is 2.5 hours, and the total extraction cycle is 10 hours. The pressure of the tail tank is 0.35-0.4MPa, and the extraction temperatures are 80°C, 90°C, 100°C, and 110°C. The extract is transported into an evaporator for concentration to obtain a crude extract concentrate with a solid mass percentage of 28.5%.
[0033] Screen out the aircraft g...
Embodiment 3
[0037] In this embodiment, the aromatic antibacterial tanning agent is prepared according to the following steps, using the aircraft grass produced in Xinhui District, Jiangmen City, Guangdong Province as raw material:
[0038] Collect the above-ground parts of the adult plants of Airplane Grass, dry and remove impurities, and crush them with a crusher. Screen out the aircraft grass material with a length of 2-10 mm and pack it into 10 m 3 In the tank, 4 tank groups are used for continuous countercurrent leaching, and water is added to the tank according to the solid-liquid mass ratio of 1:7. The extraction time of plane grass in each tank is 2.5 hours, and the total extraction cycle is 10 hours. The pressure of the tail tank is 0.35-0.4MPa, and the extraction temperatures are 80°C, 90°C, 100°C, and 110°C. The extract is transported into the evaporator for concentration to obtain a crude extract concentrate with a solid mass percentage of 30.0%.
[0039] Screen out the aircr...
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Abstract
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