Direct and reverse flotation technique for high-magnesium low-grade phosphorus ore coarse grains

A forward and reverse flotation, low-grade technology, used in flotation, solid separation and other directions, can solve the problems of long flotation time, strict environmental protection requirements, large dosage of chemicals, etc., to improve concentrate quality, high magnesium discharge rate, Low energy consumption for grinding

Active Publication Date: 2015-07-29
BLUESTAR LEHIGH ENG INST CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, with the requirements of marketization and social development, the existing problems and deficiencies of the existing technology are gradually revealed: (1) The particle size of the flotation feed is relatively fine, and the content of -200 mesh often accounts for more than 50%, resulting in a large amount of secondary mud. It not only affects the separation efficiency of flotation, but also causes a large dosage of reagents; (2) the concentration of flotation pulping is low, and the flotation time is long; The equipment is damaged, which also increases the difficulty of treating process water and cannot meet the increasingly stringent environmental protection requirements

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] Example 1, a high-magnesium and low-grade phosphate rock coarse-grained positive and negative flotation process: the high-magnesium and low-grade phosphate rock is crushed and ground, and the particle size composition of the flotation feed material is calculated by weight to meet the particle size of -200 mesh and less than 50 %, then put it in the stirring tank of the flotation machine and add water to adjust the slurry to a mass concentration higher than 50%. ), then add the positive flotation mixed collector to adjust the slurry, add water until the pulp mass concentration is 20% to carry out the positive flotation system operation, the positive flotation foam product is transferred to the reverse flotation stirring tank, and the adjusted Inorganic acid and reverse flotation mixed collector, no fresh water is added for slurry adjustment, and then fresh water is added for reverse flotation system operation, the foam product is reverse flotation tailings, discharged and...

Embodiment 2

[0017] Example 2, a high-magnesium and low-grade coarse-grained phosphate rock positive and negative flotation process: the pulp temperature is 30°C, then add regulator water glass and inorganic alkali to the pulp, and then add the positive flotation mixed collector to adjust Slurry, then add water until the pulp mass concentration is 30% to carry out the positive flotation system operation, all the other are basically the same as embodiment 1.

Embodiment 3

[0018] Example 3, a high-magnesium and low-grade coarse-grained phosphate rock positive and negative flotation process: the temperature of the pulp is 20°C, and then the regulator water glass and inorganic alkali are added to the pulp respectively, and then the positive flotation mixed collector is added for adjustment. Slurry, add water to pulp mass concentration and be 25% to carry out positive flotation system operation, all the other are basically the same as embodiment 1.

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Abstract

The invention relates to a direct and reverse flotation technique for high-magnesium low-grade phosphorus ore coarse grains. The technique comprises the following steps: crushing and grinding high-magnesium low-grade phosphorus ores; transferring into a flotation machine stirring tank and adding water for mixing slurry; keeping the temperature of the ore slurry at 10-30 DEG C, and then respectively adding regulator sodium silicate and inorganic base into the ore slurry; adding a direct flotation collecting agent for mixing the slurry; adding water for performing direct flotation system operation; transferring a direct flotation foam product into a reverse flotation stirring tank, respectively adding the regulator sodium silicate and reverse flotation mixing collecting agent into the reverse flotation stirring tank, and mixing the slurry without adding fresh water; adding fresh water and performing the reverse flotation system operation; discharging and stacking the foam products which are reverse flotation tailings, wherein the products in the tank are low-magnesium phosphorus ore concentrates; concentrating, filtering and drying, thereby acquiring the end products of concentrates. According to the technique, the last magnesium content of the concentrates is reduced and the quality of the concentrates is increased; the process is simple; the energy consumption for ore grinding is low; the dosage of agents is less; the separation effect is good; the discharging rate of magnesium is high; the water quality of concentrate and tailing is improved.

Description

technical field [0001] The invention relates to a phosphate ore beneficiation process, in particular to a high-magnesium and low-grade phosphate rock coarse-grain forward and reverse flotation process. Background technique [0002] As a non-renewable resource, phosphorus mineral is an essential chemical raw material for the production of phosphate fertilizer and phosphorus chemical products. The increasing level of social and economic development has brought about a sharp increase in the demand for phosphate rock. In my country's existing total reserves of phosphate rock, more than 90% are medium and low-grade phosphate rock, which can only be economically utilized after beneficiation and enrichment. With the depletion of easy-to-mining rich ore and easy-to-select rich ore, the research on the beneficiation technology of medium and low-grade phosphate rock is more important. For high-magnesium and low-grade phosphate rock, because the carbonate impurities are mainly dolomi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B03D1/02B03B1/04
Inventor 刘云涛刘升林钱押林刘国举刘星强
Owner BLUESTAR LEHIGH ENG INST CO LTD
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