WC-Ni mini-type component prepared based on multi-physics field activated sintering and preparing method of WC-Ni mini-type component
A technology of activating sintering and miniature parts, applied in other manufacturing equipment/tools, engine components, turbines, etc., can solve the problems of serious product pollution, low product purity, high sintering temperature, etc., achieve excellent mechanical properties, simplify the process flow, The effect of fast sintering speed
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Embodiment 1
[0032] The sample used in the experiment is a Φ4*4mm cylinder and the theoretical density of the corresponding powder is used to calculate the powder mass. WC powder and Ni powder are mixed by wet grinding method according to the weight ratio of 94:6. After weighing, put the mixed powder into the mold chuck and fix it. Under the condition of vacuum degree ≤ 0.01Pa, adjust the heating rate to 50°C / s, and simultaneously apply a force of 85MPa to both ends of the mold. When the temperature reaches 300°C, keep it warm for 80s, then adjust the heating rate to 60°C / s, when it is heated to 1150°C, keep it warm for 10 minutes, the powder is formed in the mold and sintered, and finally cooled to room temperature at a cooling rate of 15°C / s , turn off the power and take out the parts. The relative density of the sample is 98.3%, and the HV30 is kgf / mm 2 , the fracture toughness Kic is 10MPa·m1 / 2, and the product has no obvious Ni pool.
Embodiment 2
[0034] The sample used in the experiment is a Φ4*4mm cylinder and the theoretical density of the corresponding powder is used to calculate the powder mass. WC powder and Ni powder are mixed by wet grinding method according to the weight ratio of 90:10. After weighing, put the mixed powder into the mold chuck and fix it. Under the condition of vacuum degree ≤ 0.01Pa, adjust the heating rate to 25°C / s, and simultaneously apply a force of 65MPa to both ends of the mold. When the temperature reaches 180°C, keep it warm for 50s, then adjust the heating rate to 50°C / s, when heated to 1350°C, keep it warm for 8 minutes, the powder is formed in the mold and sintered, and finally cooled to room temperature at a cooling rate of 10°C / s , turn off the power and take out the parts. The relative density of the sample is 99.3%, and the HV30 is 2121kgf / mm 2 , the fracture toughness Kic is 10.1MPa m1 / 2, and the product has no obvious Ni pool.
Embodiment 3
[0036] The sample used in the experiment is a Φ4*4mm cylinder and the theoretical density of the corresponding powder is used to calculate the powder mass. WC powder and Ni powder are mixed by wet grinding method according to the weight ratio of 88:12. After weighing, put the mixed powder into the mold chuck and fix it. Under the condition of vacuum degree ≤ 0.01Pa, adjust the heating rate to 40°C / s, and simultaneously apply a force of 95MPa to both ends of the mold. When the temperature reaches 270°C, keep it warm for 100s, and then adjust the heating rate to 65°C / s. After heating to 1400°C, it is sintered 13 times in the range of 1400°C-800°C. The powder is formed in the mold and sintered, and finally Cool to room temperature at a cooling rate of 10°C / s, then turn off the power and take out the parts. The relative density of the sample is 99.5%, and the HV30 is 2096kgf / mm 2 , the fracture toughness Kic is 12.1MPa m1 / 2, and the product has no obvious Ni pool.
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