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Lily glycerol triacetate extract and application of lily glycerol triacetate extract in cigarettes

A technology of lily triacetin and triacetin, which is applied in application, tobacco, food science and other directions, can solve the problems of difficulty in cigarettes, increased production cost, limited solubility of additives, unfavorable promotion and application, etc., and achieves operability and standardization. The effect of strong sex, improving the smoking quality of cigarettes, and low cost

Inactive Publication Date: 2015-09-23
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

On the one hand, this method of adding and applying has the disadvantages of complex preparation process, limited solubility of triacetin for additives, and the difficulty of dissolving many additives that enhance flavor and sweetness of cigarettes into triacetin, which limits the Application in cigarette filter rod
On the other hand, if the filter rod is not flavored with triacetin as a medium, but the additive is directly applied to the cigarette filter rod, it will bring greater difficulty to cigarette production and significantly increase production costs, which is not conducive to large-scale production. Promoted application of

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] Wash the lily, dry it at 50°C for 10 hours, crush it to 40 mesh to obtain lily powder, weigh 5 parts of lily powder according to the weight and place it in a round bottom flask, add 15 parts of glycerol triacetate for tobacco use as an extractant After soaking at room temperature for 5 hours, reflux extraction was carried out at 80°C for 4 hours. After cooling to room temperature, the lily and triacetin after the reflux extraction were placed in microwave extraction equipment (400W, 2500MHZ), the extraction temperature is 50°C, the extraction time is 30 minutes, and the filter residue is removed by filtration to obtain a clear solution, and the desired lily triacetin extract can be obtained.

[0022] Using glyceryl triacetate as a solvent, the lily triacetin extract is formulated into a solution with a concentration of 2%, and evenly sprayed on the filter rod tow in a proportion of 7% by weight of acetate fiber tow to make a cigarette filter rod. A cigarette with a filt...

Embodiment 2

[0024] Wash the lily, dry it at 40°C for 10 hours, crush it into a 20-mesh powder, weigh 5 parts of the lily powder in parts by weight and place it in a round-bottomed flask, add 25 parts of glycerol triacetate for tobacco use as an extractant, and store it at room temperature After soaking for 8 hours, reflux extraction was carried out at 120°C for 4 hours. After cooling to room temperature, the lily and triacetin after the reflux extraction were placed in microwave extraction equipment (200W, 2500MHZ) , the extraction temperature is 60°C, the extraction time is 55 minutes, and the filter residue is removed by filtration to obtain a clear solution, and the desired lily triacetin extract can be obtained.

[0025] Using triacetin as a solvent, the lily triacetin extract is formulated into a solution with a concentration of 3%, and evenly sprayed on the filter rod tow in a proportion of 7.5% by weight of acetate fiber tow to make a cigarette filter rod. A cigarette with a filter...

Embodiment 3

[0027] Wash the lily, dry it at 45°C for 12 hours, crush it into a 10-mesh powder, weigh 5 parts of the lily powder in parts by weight and place it in a round-bottomed flask, add 20 parts of glycerol triacetate for tobacco use as an extractant, and store it at room temperature After soaking for 3 hours, reflux extraction was carried out at 80°C for 48 hours. After cooling to room temperature, the lily and triacetin after the reflux extraction were placed in a micro-extraction device (200W, 2500MHZ) , the extraction temperature is 50° C., the extraction time is 15 minutes, and the filter residue is removed by filtration to obtain a clear solution, and the desired lily triacetin extract can be obtained.

[0028] Using triacetin as a solvent, the lily triacetin extract is formulated into a solution with a concentration of 5%, and is evenly sprayed on the filter rod tow in a proportion of 7% by weight of acetate fiber tow to make a cigarette filter rod. Conventional cigarette join...

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Abstract

The invention discloses lily glycerol triacetate extract and application of the lily glycerol triacetate extract in cigarettes. Lily powder which is completely washed, dried and smashed to range from 10 meshes to 40 meshes serves as raw materials, glycerol triacetate serves as an extracting agent, firstly, extraction is conducted in a heating reflux mode, and then the lily glycerol triacetate extract is prepared through microwave extraction. The glycerol triacetate serves as a solvent, the lily glycerol triacetate extract is prepared into a solution with the concentration ranging from 2% to 5%, the solution is evenly sprayed to filter stick tows according to the 7-8% weight ratio of acetic acid fiber tows, cigarette filter sticks are prepared, and the cigarettes with the filter sticks containing effective lily components are prepared in the conventional cigarette rolling process. The extract can remarkably improve sweetness of the cigarettes, cigarette smell is abundant and coordinated, irritation and offensive odor are relieved, and the smoking quality of the cigarettes is effectively improved. The lily glycerol triacetate extract is simple in production process, high in operability and standardization and low in cost, raw materials are easy to obtain, industrial production is conveniently achieved, and good application prospects are achieved.

Description

technical field [0001] The invention belongs to the technical field of cigarette materials, and in particular relates to a lily triacetin extract. At the same time, the invention also relates to the application of the lily triacetin extract in cigarettes. Background technique [0002] Lily is sweet, slightly bitter, and slightly cold in nature. It has a sweet smell and is a precious plant resource for both medicine and food. In addition to the main starch, lily is rich in amino acids, trace elements, phospholipids, reducing sugars, steroidal saponins, flavonoids and a variety of alkaloids similar to colchicine. These ingredients work comprehensively on the human body, clearing the lungs and moistening dryness, nourishing yin and eliminating heat, clearing the heart and calming the nerves, invigorating the middle and nourishing qi, clearing heat and diuresis, detoxifying and cooling the blood, strengthening the spleen and stomach. It is a good medicine with a long history of...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24B15/26A24B3/14
CPCA24B15/26A24B3/14
Inventor 王猛张天栋颜克亮赵英良凌军
Owner CHINA TOBACCO YUNNAN IND
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