Clenbuterol hydrochloride molecularly imprinted polymer and preparation method thereof
A clenbuterol hydrochloride and molecularly imprinted technology, which is applied in the field of clenbuterol hydrochloride molecularly imprinted polymer and its preparation, can solve the problems of blurred detection line color, invisible quality control line and high missed detection rate, To achieve the effect of good blotting effect, simple and fast synthesis, and low cost
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Embodiment 1
[0025] A preparation method of clenbuterol hydrochloride molecularly imprinted polymer, comprising the following steps:
[0026] 1. The preparation concentration is 3×10 -4 The clenbuterol hydrochloride aqueous solution of mol / L;
[0027] 2. Add 5 μL of α-methacrylic acid to 20 mL at a concentration of 3 x 10 -4 mol / L clenbuterol hydrochloride aqueous solution, ultrasonic treatment for 10 minutes, then add 0.0028g N, N-methylenebisacrylamide, continue ultrasonic treatment for 20 minutes, stand overnight, to get the mixed solution (the Clenbuterol hydrochloride Tero, α-methacrylic acid, N, the molar ratio of N-methylenebisacrylamide addition is 9.78:1:3.03);
[0028] 3. Slowly add 100 μL of ammonium persulfate solution with a concentration of 0.5 mol / L to the mixed solution obtained in step 2, and ultrasonically treat it for 15 minutes to initiate a polymerization reaction to obtain a clenbuterol hydrochloride molecularly imprinted polymer.
Embodiment 2
[0030] A preparation method of clenbuterol hydrochloride molecularly imprinted polymer, comprising the following steps:
[0031] 1. The preparation concentration is 3×10 -5 The clenbuterol hydrochloride aqueous solution of mol / L;
[0032] 2. Add 3 μL of α-methacrylic acid to 10 mL to a concentration of 3 x 10 -5 mol / L clenbuterol hydrochloride aqueous solution, sonicated for 5 minutes, then added 0.0014g N,N-methylenebisacrylamide, continued sonicated for 10 minutes, left standing overnight to obtain a mixed solution (the Clenbuterol hydrochloride Tero, α-methacrylic acid, N, the molar ratio of N-methylenebisacrylamide addition is 117:1:30);
[0033] 3. Slowly add 80 μL of ammonium persulfate solution with a concentration of 0.5 mol / L to the mixed solution obtained in step 2, and ultrasonically treat for 10 minutes to initiate a polymerization reaction to obtain a clenbuterol hydrochloride molecularly imprinted polymer.
Embodiment 3
[0035] A preparation method of clenbuterol hydrochloride molecularly imprinted polymer, comprising the following steps:
[0036] 1. The preparation concentration is 3×10 -3 The clenbuterol hydrochloride aqueous solution of mol / L;
[0037] 2. Add 7 μL of α-methacrylic acid to 30 mL at a concentration of 3 x 10 -3 mol / L clenbuterol hydrochloride aqueous solution, sonicated for 15 minutes, then added 0.0042g N, N-methylenebisacrylamide, continued sonicated for 30 minutes, left standing overnight, to obtain a mixed solution (the Clenbuterol hydrochloride Tero, α-methacrylic acid, N, the molar ratio of N-methylenebisacrylamide addition is 274:300:90);
[0038] 3. Slowly add 120 μL of ammonium persulfate solution with a concentration of 0.5 mol / L to the mixed solution obtained in step 2, and ultrasonically treat it for 20 minutes to initiate a polymerization reaction to obtain a clenbuterol hydrochloride molecularly imprinted polymer.
[0039] 2. Analysis of Clenbuterol Hydrochlori...
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