Liquid-applied waterproofing membrane for roofs
A waterproof membrane and liquid technology, applied to roofs, roofs, and roof coverings using sealed aggregates, to achieve low odor characteristics, small shrinkage, and accelerated fragile time
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[0168] "Normal climate" means a temperature of 23 ± 1° C. and a relative atmospheric humidity of 50 ± 5%.
[0169] The amine content (free and hindered amines, i.e. the total content of aldimine groups) of the prepared aldimines was determined by titration (0.1N HClO in glacial acetic acid 4 , relative to crystal violet) and are given in mmol N / g.
[0170] 1. Preparation of Aldimines
[0171] Aldimine-A1: N,N'-bis(2,2-dimethyl-3-lauroyloxypropylene)-3-aminomethyl-3,5,5-trimethylcyclohexylamine
[0172] Under a nitrogen atmosphere, 598 g (2.1 mol) of 2,2-dimethyl-3-lauroyloxy-propionaldehyde were placed in a round bottom flask. Then add 170.3g (1mol) 3-aminomethyl-3,5,5-trimethylcyclohexylamine ( IPD from Evonik) followed by removal of the volatile content at 80°C and 10 mbar vacuum. This gave a yield of 732 g of an almost colorless liquid with an amine content of 2.73 mmol N / g, corresponding to a calculated aldimine equivalent weight of about 367 g / Eq.
[0173] Aldimine-...
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