Glycerol triacetate extract of figs and application of glycerol triacetate extract to cigarettes
A technology of triacetin and fig, which is applied in the application, tobacco, smoke oil filter and other directions, can solve the problems of difficulty in cigarettes, increased production cost, limited solubility of additives, complicated preparation process, etc. The effect of strong stability and standardization, and simple production process
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Embodiment 1
[0021] The figs are sliced, dried at 80°C until the water content is less than 8%, and then crushed into 40-60 mesh powder. Weigh 8 parts of fig powder according to parts by weight and place it in a round bottom flask, add 80 parts of glycerol triacetate for tobacco as an extractant, soak at room temperature for 4 hours, and carry out reflux extraction at 80°C for 10 hours. After cooling to room temperature, place the fig and triacetin mixture after reflux extraction in an ultrasonic extractor (500W, 40kHZ), extract for 40 minutes, filter and remove the filter residue to obtain a clear solution, and the desired fig triacetin can be obtained ester extract.
[0022] Using glyceryl triacetate as a solvent, the extract of fig triacetin is formulated into a solution with a concentration of 1%, and is evenly sprayed on the filter rod tow according to the weight ratio of 7% of the acetate fiber tow to make a cigarette filter rod. Cigarettes whose filter sticks contain the active ing...
Embodiment 2
[0024] Slice the figs, dry them at 60°C until the water content is less than 8%, and then crush them into 20-40 mesh powders for later use; weigh 8 parts of fig granules according to the weight and place them in a round bottom flask, add 150 parts of smoke Use glyceryl triacetate as extractant, soak at room temperature for 8 hours, then carry out reflux extraction at 100°C for 6 hours, after cooling to room temperature, place the mixture of figs and triacetin after reflux extraction in In an ultrasonic extractor (600W, 40kHZ), extract for 30 minutes, filter and remove the filter residue to obtain a clear solution, and then obtain the desired fig triacetin extract.
[0025] Using glyceryl triacetate as a solvent, the extract of fig triacetin is formulated into a solution with a concentration of 3%, and is evenly sprayed on the filter rod tow in a proportion of 8% by weight of acetate fiber tow to make a cigarette filter rod. Cigarettes whose filter sticks contain the active ing...
Embodiment 3
[0027] The figs are sliced, dried at 70°C until the water content is less than 8%, and then crushed into 20-60 mesh powder. Weigh 12 parts of fig granules according to parts by weight and place them in a round bottom flask, add 80 parts of glycerol triacetate for tobacco use as the extraction agent, soak at room temperature for 6 hours, and then carry out reflux extraction at 80°C for 4 hours , after being cooled to room temperature, the fig and triacetin mixture after the reflux extraction are placed in an ultrasonic extractor (400W, 40kHZ), extracted for 25 minutes, and a clear solution is obtained after removing the filter residue by filtration, and the required fig triacetin can be obtained. Glyceryl acetate extract.
[0028] Using triacetin as a solvent, the fig triacetin extract is formulated into a solution with a concentration of 4%, and is evenly sprayed on the filter rod tow in a proportion of 7% by weight of acetate fiber tow to make a cigarette filter rod, and pass...
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