Preparation method of weather-resistant composite for bicycle handle
A composite material and weather-resistant technology, which is applied in the field of preparation of weather-resistant composite materials for bicycle handles, can solve problems such as cracking, discoloration, and aging of bicycle handles, and achieve high elongation at break, tensile strength, and good weather resistance Effect
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Embodiment 1
[0018] (1) Modification of carbon fiber: In parts by weight, crush 25 parts of carbon fiber, add 10 parts of tartaric acid and 3 parts of epichlorohydrin, mix well, heat to 150°C, activate for 4 hours, add water to wash, remove Water phase, the organic phase is evaporated to dryness to obtain modified carbon fiber;
[0019] (2) Heat 20 parts of polyetherimide to 100°C, then add 4 parts of dicumyl peroxide, 3 parts of polystyrene particles, 2 parts of talcum powder, 1 part of hypophosphorous acid, 2 parts of diphenylamine, 5 parts of oleic acid are mixed evenly, after shearing and dispersing evenly, the modified carbon fiber prepared in step (1) is added, the temperature is raised to 140°C, and the temperature is kept for 5 hours to obtain the mixture;
[0020] (3) Put the mixture of step (2) into the internal mixer for internal mixing. The parameters of the internal mixer are 245°C in the first zone, 255°C in the second zone, 40rpm in rotation speed and 2min in residence time,...
Embodiment 2
[0022] (1) Modification of carbon fiber: in parts by weight, pulverize 40 parts of carbon fiber, add 20 parts of tartaric acid and 7 parts of epichlorohydrin, mix well, heat to 180°C, activate for 6 hours, add water to wash, remove Water phase, the organic phase is evaporated to dryness to obtain modified carbon fiber;
[0023] (2) Heat 30 parts of polyetherimide to 120°C, then add 8 parts of dicumyl peroxide, 7 parts of polystyrene particles, 4 parts of talcum powder, 3 parts of dibutyltin dilaurate, diphenylamine 4 parts and 10 parts of oleic acid are mixed evenly, after shearing and dispersing evenly, the modified carbon fiber prepared in step (1) is added, the temperature is raised to 160°C, and the temperature is kept for 8 hours to obtain the mixture;
[0024] (3) Put the mixture of step (2) into an internal mixer for internal mixing. The parameters of the internal mixer are 255°C for the first zone, 265°C for the second zone, 70rpm for the rotating speed, and 5min for t...
Embodiment 3
[0026] (1) Modification of carbon fiber: In parts by weight, crush 35 parts of carbon fiber, add 15 parts of tartaric acid and 5 parts of epichlorohydrin, mix well, heat to 170°C, activate for 5 hours, add water to wash, remove Water phase, the organic phase is evaporated to dryness to obtain modified carbon fiber;
[0027] (2) Heat 25 parts of polyetherimide to 110°C, then add 6 parts of dicumyl peroxide, 5 parts of polystyrene particles, 3 parts of talcum powder, 2 parts of hypophosphorous acid, 3 parts of diphenylamine, 8 parts of oleic acid are mixed evenly, after shearing and dispersing evenly, the modified carbon fiber prepared in step (1) is added, the temperature is raised to 150°C, and the temperature is kept for 6 hours to obtain the mixture;
[0028] (3) Put the mixture of step (2) into an internal mixer for internal mixing. The parameters of the internal mixer are 250°C for the first zone, 260°C for the second zone, 50rpm for the rotating speed, and 4min for the re...
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