Aluminum-tellurium intermediate alloy and preparing method and application thereof
An aluminum-tellurium master alloy and a master alloy technology are applied in the field of aluminum-tellurium master alloy and its preparation, which can solve the problems of tellurium segregation precipitation, difficult control, and deposition at the bottom of a crucible, etc., to achieve stable and accurate yield, and not easy to burn and oxidize , Reduce the effect of burning loss and oxidation
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Embodiment 1
[0034] The preparation method of the aluminum-tellurium master alloy described in this embodiment is as follows:
[0035] (1) Ingredients
[0036] Using tellurium and aluminum as raw materials, the mass fraction of tellurium in the aluminum-tellurium master alloy is 0.1%, and the mass fraction of aluminum is 99.9% to weigh the raw materials;
[0037] (2) Melting
[0038] After preheating aluminum in a heating furnace to remove adsorbed moisture and gas, add a covering agent of 0.5% of the total mass of aluminum and tellurium, the covering agent is obtained by mixing sodium chloride and potassium chloride at a mass ratio of 1:1 The mixture is heated to melt all the aluminum to obtain aluminum liquid, and then the tellurium is pressed into the aluminum liquid in batches with a bell jar at 680 ° C. The amount added each time is 3% of the total amount of tellurium. After all the tellurium is added and melted, Keep stirring at 680°C for 5 minutes, then remove slag, keep the tempe...
Embodiment 2
[0042] The preparation method of the aluminum-tellurium master alloy described in this embodiment is as follows:
[0043] (1) Ingredients
[0044] Using tellurium and aluminum as raw materials, the mass fraction of tellurium in the aluminum-tellurium master alloy is 1.0%, and the mass fraction of aluminum is 99.0% to weigh the raw materials;
[0045] (2) Melting
[0046]Put the aluminum in a heating furnace to preheat to remove the adsorbed moisture and gas, add potassium chloride as a covering agent of 1.0% of the total mass of aluminum and tellurium, heat to melt all the aluminum to obtain aluminum liquid, and then heat it in batches at 720°C Press tellurium into molten aluminum with a bell jar, adding 5% of the total amount of tellurium each time. After all the tellurium is added and melted, keep stirring at 700°C for 10 minutes and remove slag. Keep the temperature at 700°C. Add 0.7% refining agent carbon tetrachloride to the aluminum and tellurium melt after slag, stir ...
Embodiment 3
[0050] The preparation method of the aluminum-tellurium master alloy described in this embodiment is as follows:
[0051] (1) Ingredients
[0052] Using tellurium and aluminum as raw materials, the mass fraction of tellurium in the aluminum-tellurium master alloy is 10.0%, and the mass fraction of aluminum is 90.0% to weigh the raw materials;
[0053] (2) Melting
[0054] Put the aluminum in a heating furnace to preheat to remove the adsorbed moisture and gas, add potassium chloride as a covering agent of 1.0% of the total mass of aluminum and tellurium, heat to melt all the aluminum to obtain aluminum liquid, and then heat it in batches at 720°C Press tellurium into molten aluminum with a bell jar, adding 5% of the total amount of tellurium each time. After all the tellurium is added and melted, keep stirring at 700°C for 10 minutes and remove slag. Keep the temperature at 700°C. Add 0.7% refining agent carbon tetrachloride to the aluminum and tellurium melt after slag, sti...
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