Flexible symmetrical pseudocapacitance super capacitor and preparation method thereof
A supercapacitor, symmetrical technology, applied in the manufacture of hybrid/electric double layer capacitors, hybrid capacitor electrodes, hybrid capacitor collectors, etc., can solve the problems of distinguishing polarity, inconvenient use, etc., to increase the load capacity, fast Effect of charge and discharge, large pseudocapacitance specific capacity
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Embodiment 1
[0033] Preparation of nano-nickel particles / multi-walled carbon nanotubes / conductive carbon cloth electrode, the preparation method includes: using an electrochemical workstation three-electrode system, using carbon fiber cloth as a working electrode, metal platinum sheet as a counter electrode, and calomel as a reference electrode . In a sulfuric acid solution of 1 mole per liter, it was polarized at a constant potential at a positive potential of 2.5 volts for 10 minutes, and the carbon fiber cloth was taken out and dried in an electric blast drying oven to obtain a treated hydrophilic conductive carbon cloth. 2.9 grams of nickel nitrate (Ni(NO 3 ) 2 ·6H 2O) dissolved in 50 ml of water (H 2 O) in the solution, stir with a magnetic stirrer to make it fully dissolve, mix evenly, and make a solution; cut out the treated conductive carbon cloth, place it in the prepared nickel nitrate solution for soaking, take it out, and dry it at 100 degrees Celsius 1 hour; under an inert...
Embodiment 2
[0040] The preparation of nano-nickel particles / multi-walled carbon nanotubes / conductive carbon cloth electrodes, the preparation method includes: in the electrochemical workstation three-electrode system, carbon fiber cloth is used as the working electrode, metal platinum sheet is used as the counter electrode, and calomel is used as the reference electrode . In a sulfuric acid solution of 2 moles per liter, use the constant potential polarization mode, and polarize at a positive potential of 3 volts for 5 minutes, take out the carbon fiber cloth and dry it in an electric blast drying oven to obtain the treated hydrophilic conductive carbon cloth . 1.5 grams of nickel nitrate (Ni(NO 3 ) 2 ·6H 2 O) dissolved in 50 ml of water (H 2 O) in the solution, stir with a magnetic stirrer to make it fully dissolve, mix evenly, and make a solution; cut the conductive carbon cloth after the activation treatment and place it in the nickel nitrate solution that has been prepared for inf...
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