This invention relates to the field of
inorganic materials, specifically to a method for preparing low-lead
antimony trioxide. The method involves crushing
antimony ingots, first melting and oxidizing them, then distilling to remove impurities to obtain a refined product. The refined product,
organic acid, and
polyol are mixed, heated, and reacted, followed by
filtration to remove insoluble matter, yielding an
antimony complex solution. A long-chain organic amine is dissolved in a mixed
solvent of
anhydrous ethanol and deionized water to obtain a long-chain organic amine solution. The antimony complex solution is added to the long-chain organic amine solution, and the pH is adjusted to 6-7. The reaction solution is transferred to a hydrothermal reactor, sealed, and subjected to
hydrothermal reaction. The precipitate is collected, washed, and dried. The resulting
nanosheet-like clustered
antimony trioxide exhibits high purity, low
impurity content, extremely high specific surface area, abundant active sites,
high energy density, and good cycle performance, making it a highly promising
pseudocapacitor electrode material.