Method for continuously measuring contents of calcium and magnesium in silicon, calcium, barium and magnesium alloy
A determination method and technology of magnesium alloys are applied in the direction of material analysis by observing the influence of chemical indicators, and analysis by chemical reaction of materials, etc., which can solve the problems of waste of reagents, cumbersome operation and high cost, and improve production. Efficiency, shorten the operation process, reduce the effect of inspection cost
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[0033] The above and other technical features and advantages of the present invention will be described in more detail below in conjunction with the embodiments.
[0034] 1. Method summary: Use nitric acid (67%)-hydrofluoric acid (40%) to dissolve the sample in a polyethylene plastic beaker, add perchloric acid (70%) to produce smoke, the smoke will be clean, no smoke can be seen, try The liquid dries up. Add 10 mL of hydrochloric acid (65%), and heat to dissolve the salts. Transfer the test solution to a 250mL volumetric flask and dilute to a constant volume. Divide two 50mL solutions into two 250mL beakers, add 50mL triethanolamine (12%) to one portion, add 50mL water, add a little hydroxylamine hydrochloride, and add 30mL potassium hydroxide solution (20%, keep pH not low In 12), appropriate amount of calcein, titrate with EDTA standard solution until the fluorescence green disappears as the end point; add 50mL triethanolamine (12%), add 50mL water, add a little hydroxylamin...
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