High-toughness antibacterial sports protective device and preparing method thereof
A sports protective gear and high toughness technology, applied in the field of high toughness antibacterial sports protective gear, can solve the problems of lack of targeted technology integration in immunity, health care, and sterilization, and achieve good synergy, high content of active ingredients, and long validity period Effect
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Embodiment 1
[0033] A preparation method of high-toughness antibacterial sports protective gear, comprising the following steps:
[0034] Step 1. Prepare a mixed solution of concentrated sulfuric acid, concentrated nitric acid and potassium permanganate according to the ratio of 10mL: 3mL: 20g, add graphite powder into the mixed solution according to the ratio of 1g: 20mL, heat in a water bath and stir until the temperature reaches At 45°C, according to the ratio of mixed solution: deionized water: hydrogen peroxide = 2:1:0.5, add deionized water and hydrogen peroxide in sequence, after stirring for 30 minutes, let it stand still, take out the precipitate, and place the precipitate in deionized water to obtain Mother liquor: According to the ratio of 10mL: 1.5g: 5mL, take the mother liquor, ferrous sulfate and concentrated ammonia water in sequence, mix them and disperse them ultrasonically for 50 minutes, then heat them in a water bath at 97°C for 30 minutes, centrifuge to separate the pre...
Embodiment 2
[0041] A preparation method of a high-toughness antibacterial sports protective gear, comprising the following steps: Step 1. Concentrated sulfuric acid, concentrated nitric acid and potassium permanganate are prepared into a mixed solution according to the ratio of 10mL: 3mL: 20g, and according to the ratio of 1g: 20mL, Add graphite powder into the mixed solution, heat in a water bath and stir until the temperature reaches 45°C. According to the ratio of mixed solution: deionized water: hydrogen peroxide = 2:1:0.5, add deionized water and hydrogen peroxide in sequence. After stirring for 20 minutes, stand still. Place, remove the precipitate, and place the precipitate in deionized water to obtain the mother liquor; according to the ratio of 10mL: 1.5g: 5mL, take the mother liquor, ferrous sulfate and concentrated ammonia water in sequence, mix and ultrasonically disperse for 30min, and then in 90℃ Heated in a water bath for 30 minutes, centrifuged to obtain a precipitate, wash...
Embodiment 3
[0048] A preparation method of a high-toughness antibacterial sports protective gear, comprising the following steps: Step 1. Concentrated sulfuric acid, concentrated nitric acid and potassium permanganate are prepared into a mixed solution according to the ratio of 10mL: 3mL: 20g, and according to the ratio of 1g: 20mL, Add graphite powder into the mixed solution, heat and stir in a water bath until the temperature reaches 45°C, add deionized water and hydrogen peroxide in sequence according to the ratio of mixed solution: deionized water: hydrogen peroxide = 2:1:0.5, and stir for 20-35 minutes After standing still, the precipitate was taken out, and the precipitate was placed in deionized water to obtain the mother liquor; according to the ratio of 10mL: 1.5g: 5mL, the mother liquor, ferrous sulfate and concentrated ammonia water were taken in sequence, and after mixing, ultrasonic dispersion was carried out for 60min, and then in 100 Heating in a water bath at ℃ for 30 minut...
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Abstract
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