Method for synthesizing CHA molecular sieve by using tetraethyl ammonium hydroxide as templating agent
A technology of tetraethylammonium hydroxide and molecular sieves, which is applied in chemical instruments and methods, molecular sieves and alkali exchange compounds, inorganic chemistry, etc., can solve the problems of high price and low solid phase yield, and achieve pollution reduction and solid phase The effect of high yield and reduced production cost
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Embodiment 1
[0013] Embodiment 1: Using tetraethylammonium hydroxide as a template to synthesize CHA molecular sieves, the steps are as follows:
[0014] First, 16.8296g template agent tetraethylammonium hydroxide (TEAOH, 35wt%) is mixed with 1.6004g NaOH solid; Then, take 12.9874g commercially available USY molecular sieve (USY zeolite is used as silicon source and aluminum source to synthesize aluminosilicate molecular sieve, This embodiment selects CBV-720, molar ratio SiO 2 / Al 2 o 3 =30) was added to the mixture as a silicon source and an aluminum source; continued stirring until a homogeneous gel was obtained;
[0015] Transfer the gel to a stainless steel, polytetrafluoroethylene-lined autoclave, and conduct hydrothermal crystallization at 160°C for 3 days under static conditions; the gel ratio of the system is: SiO 2 / 0.033Al 2 o 3 / 0.2TEAOH / 0.2NaOH / 5H 2 O. After the reaction, cool at room temperature, filter the product, wash with deionized water, and dry at 100°C for 12 ho...
Embodiment 2
[0016] Example 2: Using tetraethylammonium hydroxide as a template to synthesize CHA molecular sieve, the basic steps are the same as in Example 1, except that the crystallization condition is 3 days at 140° C. to finally obtain SSZ-13 molecular sieve.
Embodiment 3
[0017] Example 3: Using tetraethylammonium hydroxide as a template to synthesize CHA molecular sieves, the basic steps are the same as in Example 1, except that the crystallization conditions are crystallization at 160° C. for 4 days, and finally SSZ-13 molecular sieves are obtained.
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