Method for detecting ferric ions by using fluorescent carbon quantum dots
A technology of carbon quantum dots and ferric iron, applied in the field of using fluorescent carbon quantum dots to detect ferric ions, can solve the problems of poor selectivity, complicated preparation and processing processes, and the inability to detect Fe alone, and achieve the effect of convenient operation
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[0024] Example 1
[0025] (1) Prepare a dispersion with a mass ratio of glucose and absolute ethanol of 5:1;
[0026] (2) Place the above-mentioned mixed solution in a hydrothermal reaction vessel, and place the hydrothermal reaction vessel in an environment at 150° C. for 18 hours to react to obtain fluorescent quantum dots.
[0027] (3) Add 1 ml of the above carbon quantum dot solution to 8 quartz fluorescent cuvettes;
[0028] (4) Use a pipette to adjust the concentration to 0; 2×10 -8 ; 4×10 -8 ; 2×10 -7 ; 8×10 -7 ; 2×10 -6 ; 6×10 -6 ; 4×10 -5 The FeCl3 solution was added to the cuvette containing carbon quantum dots, and put it into the fluorescence spectrophotometer;
[0029] (5) After testing the optimal excitation wavelength of the carbon quantum dots at 360 nm, and adjusting the excitation wavelength of the fluorescence spectrophotometer to the excitation wavelength, recording the curve of the fluorescence intensity of the solution with the fluorescence emission wavelength.
[0...
Example
[0035] Example (2)
[0036] (1) Prepare a dispersion liquid with a mass ratio of glucose and absolute ethanol of 15:1, and place it in a hydrothermal reactor;
[0037] (2) Put the above-mentioned sealed hydrothermal reaction kettle in an environment at 150°C for 18 hours to obtain the carbon quantum dots to be synthesized, such as figure 1 , 2 Shown from figure 1 , figure 2 It can be seen that the size of the prepared carbon quantum dots is below 6nm, from figure 2 It can be seen that 60% of the carbon quantum dots prepared by the present invention are 3-5nm in size;
[0038] (3) Add 1 ml of the above carbon quantum dot solution to 14 quartz fluorescent cuvettes;
[0039] (4) Use a pipette to adjust the concentration to 0; 2×10 -8 ; 4×10 -8 ; 6×10 -8 ; 2×10 -7 ; 4×10 -7 ; 6×10 -7 ; 8×10 -7 ; 2×10 -6 ; 4×10 -6 ; 6×10 -6 ; 2×10 -5 ; 4×10 -5 ; 6×10 -5 The FeCl3 solution was added to the cuvette containing carbon quantum dots, and put it into the fluorescence spectrophotometer;
[0040] (...
Example Embodiment
[0047] Example 3
[0048] (1) Prepare a 25:1 dispersion liquid with a mass ratio of glucose and absolute ethanol, and place it in a hydrothermal reactor for sealing;
[0049] (2) Put the above-mentioned sealed hydrothermal reactor in an environment at 180°C for 18 hours to obtain the carbon quantum dots to be synthesized;
[0050] (3) Add 1 ml of the above carbon quantum dot solution to 14 quartz fluorescent cuvettes;
[0051] (4) Use a pipette to adjust the concentration to 0; 2×10 -8 ; 4×10 -8 ; 6×10 -8 ; 8×10 -8 ; 2×10 -7 ; 4×10 -7 ; 6×10 -7 ; 8×10 -7 ; 2×10 -6 ; 4×10 -6 ; 6×10 -6 ; 2×10 -5 ; 4×10 -5 The FeCl3 solution was added to the cuvette containing carbon quantum dots, and put it into the fluorescence spectrophotometer;
[0052] (5) After testing, the optimal excitation wavelength of the fluorescent carbon quantum dot solution in the present invention is 360 nm, so adjust the excitation wavelength of the fluorescence spectrophotometer to 360 nm, and record the curve of the fluo...
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