Anti-macroglobulin monoclonal antibody hybridoma cell line
A hybridoma cell line and monoclonal antibody technology, applied in the field of hybridoma cell line and its preparation, can solve problems such as low activity and recovery rate
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[0036] 1) Preparation of immune antigen:
[0037] Dissolve 1 mg of human macroglobulin in 0.25 mL DMSO solution, add EDC, shake vigorously for 2 hours at room temperature and avoid light, and react overnight at 4°C. Add the above solution slowly and dropwise to the BSA solution and shake for 2 hours at room temperature away from light. In 0.05molL -1 After 72 hours of dialysis against light in PBS buffer, a conjugate of macroglobulin and carrier protein BSA was obtained.
[0038] 2) Mouse immunity:
[0039] Using human macroglobulin-BSA conjugate as the immune antigen, immunize 7-week-old female Balb / c mice, and mix it with Freund’s complete adjuvant at a volume ratio of 1:1 at a dose of 100 μg / mouse. Emulsify to a water-in-oil state, immunize Balb / c mice with the emulsified complete antigen and subcutaneously inject at multiple points on the back of the neck. After 2 weeks, emulsify with the same antigen and an equal volume of Freund’s incomplete adjuvant, 100μg / only for boost Imm...
Embodiment
[0050] 1. Materials and instruments
[0051] 1.1 Cell lines, tissue specimens and animals
[0052] a. Myeloma cells (SP2 / 0): from ATCC (American Type Culture Collection).
[0053] b. Balb / c mice: purchased from the animal platform of Tsinghua University.
[0054] 1.2 Main reagents
[0055] a. Freund's complete adjuvant, Freund's incomplete adjuvant, HAT, HT, TMB, PEG (molecular weight 4000), EDC: purchased from Sigma;
[0056] b. HRP-labeled goat anti-mouse IgG: purchased from Gibco;
[0057] c. RPMI1640 medium: purchased from HyClone;
[0058] d. Cellulose acetate membrane (NC): purchased from Hybond;
[0059] e. Fetal bovine serum: purchased from PAN Company;
[0060] f. Murine monoclonal antibody subtype typing kit: purchased from Thermo Branch;
[0061] g. Coating buffer: 0.795g sodium carbonate and 1.465g sodium bicarbonate are added to each 500ml deionized water, and the pH is 9.6.
[0062] h. Substrate buffer: Add 9.2g of disodium hydrogen phosphate dodecahydrate and 2.55g of citric aci...
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