Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Preparation method of flame-retardant PET fiber

A fiber and carbon-coated technology, which is applied in the manufacture of fire-retardant and flame-retardant filaments, fiber processing, melt spinning, etc. Dispersibility and compatibility, droplet and smoke reduction, effect of improving flame retardancy

Active Publication Date: 2016-03-16
TAIYUAN UNIV OF TECH
View PDF5 Cites 7 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, PET has a low limiting oxygen index and is a flammable fiber, which makes it a huge safety hazard in its application.
[0004] At present, all parts of the world are competing to develop PET flame-retardant products, but the existing flame-retardant PETs often have the following problems in practical applications: some flame-retardant PETs will produce thick smoke and toxic and harmful gases when burned; some flame-retardant PETs have Excellent flame retardant and smoke suppression functions, but the mechanical properties of the material itself have dropped too much, and it is difficult to form fibers, which is difficult to meet the actual use requirements
However, the flame retardant also has the problem that the spinnability of the fiber will be deteriorated and the mechanical properties of the spun fiber will be reduced.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Preparation method of flame-retardant PET fiber
  • Preparation method of flame-retardant PET fiber
  • Preparation method of flame-retardant PET fiber

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0019] The following embodiments are only preferred technical solutions of the present invention, and are not used to limit the present invention in any way. For those skilled in the art, the present invention can have various modifications and changes. Any modification, equivalent replacement, improvement, etc., made within the spirit and principle of the present invention shall be included in the protection scope of the present invention.

[0020] Add 10 g of carbon microspheres to 100 mL of absolute ethanol, and disperse for 10 minutes with ultrasonic waves at a frequency of 40 KHz to obtain a suspension of carbon microspheres.

[0021] The above-mentioned carbon microsphere suspension was added to 300 mL ammonia water, heated to 40° C. with stirring, and 500 mL of 0.4 mol / L magnesium chloride aqueous solution was dropped at a dropping rate of 3 mL / min. After the addition, the stirring was continued for 2 hours. The reactants were taken out and washed with absolute ethanol and ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
diameteraaaaaaaaaa
particle sizeaaaaaaaaaa
limiting oxygen indexaaaaaaaaaa
Login to View More

Abstract

The invention relates to a preparation method of flame-retardant PET fiber. The preparation method comprises the following steps: first, wrapping a magnesium hydroxide coated carbon microsphere flame retardant with a PET layer to obtain an encapsulated magnesium hydroxide coated carbon microsphere flame retardant, so as to effectively improve the dispersity and the compatibility of the flame retardant in a polymer substrate, and improve the spinnability of a material; second, adding 1 wt% of the encapsulated magnesium hydroxide coated carbon microsphere flame retardant in the preparation process of PET fiber, carrying out melt blending and spinning to prepare magnesium hydroxide coated carbon microsphere / polyethylene glycol terephthalate fiber, and adjusting the melt blending and spinning technology reasonably to further improve the spinnability of the flame-retardant PET fiber. The flame-retardant PET fiber prepared according to the preparation method has the advantages that not only is the flame retardant property improved, but also the own physical and chemical properties of fiber are prevented from being damaged; the limited oxygen index of the obtained fiber can reach up to 30 percent or higher; the molten drop quantity and the smoke quantity are greatly reduced; the mechanical property and the hygroscopicity are favorable; requirements of environmental protection and practical use are met.

Description

Technical field [0001] The invention belongs to the technical field of functional fiber preparation, and relates to a preparation method of flame-retardant polyethylene terephthalate fiber. Background technique [0002] According to foreign sources, half of the fires are caused by textiles. [0003] Polyethylene terephthalate fiber, referred to as PET fiber, commonly known as polyester, has the advantages of excellent mechanical properties, non-toxic and odorless, good hygiene and safety, oil resistance, gas barrier, etc., and it is the most widely used chemical fiber at present. one. However, PET has a low limiting oxygen index and is a flammable fiber, making it a huge safety hazard in its application. [0004] At present, all parts of the world are competing to develop PET flame-retardant products, but the existing flame-retardant PET often has the following problems in practical applications: some flame-retardant PET will produce dense smoke and toxic and harmful gases when bur...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): D01F6/92D01F1/07D01D5/08D01D5/088D01D5/16D01D10/02
Inventor 牛梅杨雅茹李京京薛宝霞戴晋明王淑花侯文生
Owner TAIYUAN UNIV OF TECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products